1-Allylcyclopropanesulfonic acid potassium salt

Base Information

• Chemical Name: 1-Allylcyclopropanesulfonic acid potassium salt
• CAS No.: 923032-57-9
• Molecular Formula: C6H10O3S.K
• Molecular Weight: 200.30
• Mol file: 923032-57-9.mol

Synonyms:(1-Allylcyclopropyl)sulfonyloxypotassium;

Chemical Property of 1-Allylcyclopropanesulfonic acid potassium salt

Chemical Property:

• PSA: 65.58000
• LogP: 1.72110
• Solubility.: Water

Purity/Quality:

98%Min ^*data from raw suppliers

1-Allylcyclopropanesulfonic acid potassium salt ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Allylcyclopropanesulfonic acid potassium salt

There total 2 articles about 1-Allylcyclopropanesulfonic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

butyl 1-allylcyclopropane-1-sulfonate (923032-56-8) → potassium 1-allylcyclopropane-1-sulfonate (923032-57-9)

Guidance literature:

With water; potassium thioacyanate; In 1,2-dimethoxyethane; for 16h; Heating / reflux;

Reference yield:

butyl 1-methylcyclopropane-1-sulfonate (923032-53-5) → potassium 1-allylcyclopropane-1-sulfonate (923032-57-9)

Guidance literature:

With potassium thioacyanate; In 1,2-dimethoxyethane; water;

Reference yield: 87.0%

potassium 1-allylcyclopropane-1-sulfonate (923032-57-9) → 1-allylcyclopropane-1-sulfonyl chloride (923032-59-1)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; for 16h; Heating / reflux;

upstream raw materials:

butyl 1-allylcyclopropane-1-sulfonate

butyl 1-methylcyclopropane-1-sulfonate

Downstream raw materials:

1-allylcyclopropane-1-sulfonyl chloride

1-allyl-N-(3,4-difluoro-2-(2-fluoro-4-iodophenylamino)phenyl)cyclopropane-1-sulfonamide

1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

Refernces

• 1、 -. "COMBINATIONS OF MEK INHIBITORS AND RAF KINASE INHIBITORS AND USES THEREOF". . . Retrieved 2012/06/16.
• 2、 -. "N-(ARYLAMINO)-SULFONAMIDE INHIBITORS OF MEK". Page/Page column 52. . Retrieved 2008/06/13.