1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

Base Information

Chemical Name:1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide
CAS No.:923032-78-4
Molecular Formula:C₁₈H₁₅F₄IN₂O₂S
Molecular Weight:526.293
Hs Code.:

Synonyms:1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

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Chemical Property of 1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

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Technology Process of 1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

There total 4 articles about 1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923032-59-1
1-allylcyclopropane-1-sulfonyl chloride

: 765962-72-9
3,4,6-trifluoro-N₁-2-(2-fluoro-4-iodophenyl)benzene-1,2-diamine

: 923032-78-4
1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

Guidance literature:: With pyridine; at 40 ℃; for 48h;

Reference yield:

: 923032-56-8
butyl 1-allylcyclopropane-1-sulfonate

: 923032-78-4
1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium thioacyanate / 1,2-dimethoxyethane; water / 16 h / Reflux

2: thionyl chloride / N,N-dimethyl-formamide / 16 h / 60 °C / Reflux

3: pyridine / 48 h / 40 °C

With pyridine; thionyl chloride; potassium thioacyanate; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;

Reference yield:

: 923032-57-9
potassium 1-allylcyclopropane-1-sulfonate

: 923032-78-4
1-allyl-cyclopropanesulfonic acid [3,4,6-trifluoro-2-(2-fluoro-4-iodo-phenylamino)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 16 h / 60 °C / Reflux

2: pyridine / 48 h / 40 °C

With pyridine; thionyl chloride; In N,N-dimethyl-formamide;