4-Quinazolinecarbonyl chloride, 2-phenyl-

Base Information

Chemical Name:4-Quinazolinecarbonyl chloride, 2-phenyl-
CAS No.:92309-78-9
Molecular Formula:C15H9ClN2O
Molecular Weight:268.702
Hs Code.:

Synonyms:

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Chemical Property of 4-Quinazolinecarbonyl chloride, 2-phenyl-

Chemical Property:

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Technology Process of 4-Quinazolinecarbonyl chloride, 2-phenyl-

There total 6 articles about 4-Quinazolinecarbonyl chloride, 2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7672-01-7
2-phenylquinazoline-4-carboxylic acid

: 92309-78-9
2-Phenyl-quinazoline-4-carbonyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm960818o

Reference yield:

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 92309-78-9
2-Phenyl-quinazoline-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 3 h / Heating

2: SnCl₄ / 1,2-dichloro-benzene / 0.25 h / 140 °C

3: 20percent NaOH / aq. ethanol / 2 h / Heating

4: oxalyl chloride, DMF / CH₂Cl₂ / 2 h / 0 - 20 °C

With sodium hydroxide; thionyl chloride; oxalyl dichloride; tin(IV) chloride; N,N-dimethyl-formamide; In ethanol; dichloromethane; 1,2-dichloro-benzene;
DOI:10.1021/jm960818o

Reference yield:

: 92566-52-4
ethyl 2-phenylquinazoline-4-carboxylate

: 92309-78-9
2-Phenyl-quinazoline-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 20percent NaOH / aq. ethanol / 2 h / Heating

2: oxalyl chloride, DMF / CH₂Cl₂ / 2 h / 0 - 20 °C

With sodium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1021/jm960818o