(2E)-5-[(3-methoxyphenyl)hydrazono]-4-phenyl-1,3-thiazol-2(5H)-imine

Base Information

• Chemical Name: (2E)-5-[(3-methoxyphenyl)hydrazono]-4-phenyl-1,3-thiazol-2(5H)-imine
• CAS No.: 26179-13-5
• Molecular Formula: C₁₆H₁₄N₄OS
• Molecular Weight: 310.379

Synonyms:2-Thiazolamine,5-[(3-methoxyphenyl)azo]-4-phenyl- (9CI); Thiazole,2-amino-5-[(m-methoxyphenyl)azo]-4-phenyl- (8CI); NSC 125408

Chemical Property of (2E)-5-[(3-methoxyphenyl)hydrazono]-4-phenyl-1,3-thiazol-2(5H)-imine

Chemical Property:

• Vapor Pressure: 4.28E-08mmHg at 25°C
• Boiling Point: 444.4°Cat760mmHg
• Flash Point: 222.6°C
• Density: 1.31g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E)-5-[(3-methoxyphenyl)hydrazono]-4-phenyl-1,3-thiazol-2(5H)-imine

There total 1 articles about (2E)-5-[(3-methoxyphenyl)hydrazono]-4-phenyl-1,3-thiazol-2(5H)-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Amino-4-phenylthiazole (2010-06-2) + m-Anisidine (536-90-3,918666-97-4) → 5-(3-methoxy-phenylazo)-4-phenyl-thiazol-2-ylamine (26179-13-5)

Guidance literature:

Multistep reaction; (i) NaNO₂, aq. HCl, (ii) /BRN= 128609/, NaOAc, EtOH;

DOI:10.1002/jps.2600590316

Reference yield: 50.0%

4-nitrobenzaldehdye (555-16-8) + 5-(3-methoxy-phenylazo)-4-phenyl-thiazol-2-ylamine (26179-13-5) → [5-(3-Methoxy-phenylazo)-4-phenyl-thiazol-2-yl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Guidance literature:

With piperidine; In ethanol; for 3h; Heating;

Reference yield: 50.0%

5-(3-methoxy-phenylazo)-4-phenyl-thiazol-2-ylamine (26179-13-5) + 2-nitro-benzaldehyde (552-89-6) → [5-(3-Methoxy-phenylazo)-4-phenyl-thiazol-2-yl]-[1-(2-nitro-phenyl)-meth-(E)-ylidene]-amine

Guidance literature:

With piperidine; In ethanol; for 3h; Heating;

upstream raw materials:

2-Amino-4-phenylthiazole

m-Anisidine

Downstream raw materials:

1-[5-(3-methoxy-phenylazo)-4-phenyl-thiazol-2-yl]-3-phenyl-thiourea

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