3-Pyrrolidinecarboxylic acid, 1-(6-chloro-3-pyridazinyl)-4-(2,4-difluorophenyl)-, lithium salt (1:1), (3S,4R)-

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Chemical Name:3-Pyrrolidinecarboxylic acid, 1-(6-chloro-3-pyridazinyl)-4-(2,4-difluorophenyl)-, lithium salt (1:1), (3S,4R)-
CAS No.:923948-67-8
Molecular Formula:C15H12ClF2N3O2.Li
Molecular Weight:345.662
Hs Code.:

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Chemical Property of 3-Pyrrolidinecarboxylic acid, 1-(6-chloro-3-pyridazinyl)-4-(2,4-difluorophenyl)-, lithium salt (1:1), (3S,4R)-

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Technology Process of 3-Pyrrolidinecarboxylic acid, 1-(6-chloro-3-pyridazinyl)-4-(2,4-difluorophenyl)-, lithium salt (1:1), (3S,4R)-

There total 1 articles about 3-Pyrrolidinecarboxylic acid, 1-(6-chloro-3-pyridazinyl)-4-(2,4-difluorophenyl)-, lithium salt (1:1), (3S,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 923948-66-7
methyl (3S,4R)-1-(6-chloropyridazin-3-yl)-4-(2,4-difluorophenyl)pyrrolidine-3-carboxylate

: 923948-67-8
lithium (3S,4R)-1-(6-chloropyridazin-3-yl)-4-(2,4-difluorophenyl)pyrrolidine-3-carboxylate

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 16h;

Reference yield: 62.0%

: 923948-67-8
lithium (3S,4R)-1-(6-chloropyridazin-3-yl)-4-(2,4-difluorophenyl)pyrrolidine-3-carboxylate

: 923948-68-9
(3S,4R)-4-(2,4-difluorophenyl)-1-pyridazin-3-ylpyrrolidine-3-carboxylic acid hydrochloride

Guidance literature:: lithium (3S,4R)-1-(6-chloropyridazin-3-yl)-4-(2,4-difluorophenyl)pyrrolidine-3-carboxylate; With 2,5-dihydrotoluene; palladium 10% on activated carbon; In ethanol; for 4h; Heating / reflux;

With hydrogenchloride; In diethyl ether; water; acetone;