3-Quinolinecarboxylic acid, 2-methyl-6-phenyl-

Base Information

Chemical Name:3-Quinolinecarboxylic acid, 2-methyl-6-phenyl-
CAS No.:92513-33-2
Molecular Formula:C17H13NO2
Molecular Weight:263.296
Hs Code.:

Synonyms:

Suppliers and Price of 3-Quinolinecarboxylic acid, 2-methyl-6-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 6 raw suppliers

Chemical Property of 3-Quinolinecarboxylic acid, 2-methyl-6-phenyl-

Chemical Property:

Purity/Quality:: 95+% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Quinolinecarboxylic acid, 2-methyl-6-phenyl-

There total 4 articles about 3-Quinolinecarboxylic acid, 2-methyl-6-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1426814-54-1
4-aminobiphenyl-3-carbaldehyde

: 141-97-9
ethyl acetoacetate

: 92513-33-2
6-phenyl-2-methylquinoline-3-carboxylic acid

Guidance literature:: 4-aminobiphenyl-3-carbaldehyde; ethyl acetoacetate; With toluene-4-sulfonic acid; at 100 ℃; for 0.166667h;

With sodium hydroxide; In water; for 2h; Reflux;
DOI:10.3390/molecules17055497

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 92513-33-2
6-phenyl-2-methylquinoline-3-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: violet acid / -5 - 20 °C

2.1: palladium diacetate; potassium carbonate; acetylacetone / ethanol / 1 h / Reflux

3.1: ammonium chloride; zinc / ethanol; water / 2 h / 20 °C

4.1: toluene-4-sulfonic acid / 0.17 h / 100 °C

4.2: 2 h / Reflux

With violet acid; palladium diacetate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; acetylacetone; zinc; In ethanol; water; 2.1: Suzuki coupling;
DOI:10.3390/molecules17055497

Reference yield:

: 20357-20-4
5-bromo-2-nitrobenzaldehyde

: 92513-33-2
6-phenyl-2-methylquinoline-3-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium diacetate; potassium carbonate; acetylacetone / ethanol / 1 h / Reflux

2.1: ammonium chloride; zinc / ethanol; water / 2 h / 20 °C

3.1: toluene-4-sulfonic acid / 0.17 h / 100 °C

3.2: 2 h / Reflux

With palladium diacetate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; acetylacetone; zinc; In ethanol; water; 1.1: Suzuki coupling;
DOI:10.3390/molecules17055497