Cyclohexaneacetic acid, 1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-, 3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo hexyl]oxy]-2,2-dimethylpropyl ester

Base Information

Chemical Name:Cyclohexaneacetic acid, 1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-, 3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo hexyl]oxy]-2,2-dimethylpropyl ester
CAS No.:925237-15-6
Molecular Formula:C₃₂H₅₈N₂O₈
Molecular Weight:598.821
Hs Code.:

Cyclohexaneacetic acid,
1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-,
3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo
hexyl]oxy]-2,2-dimethylpropyl ester

Synonyms:

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Chemical Property of Cyclohexaneacetic acid, 1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-, 3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo hexyl]oxy]-2,2-dimethylpropyl ester

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Technology Process of Cyclohexaneacetic acid, 1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-, 3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo hexyl]oxy]-2,2-dimethylpropyl ester

There total 3 articles about Cyclohexaneacetic acid, 1-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-, 3-[[(3S)-3-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]-5-methyl-1-oxo hexyl]oxy]-2,2-dimethylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925236-95-9
[1-(tert-butoxycarbonylamino-methyl)-cyclohexyl]-acetic acid 3-hydroxy-2,2-dimethyl-propyl ester

: 649748-09-4
(S)-3-(((tert-butoxycarbonyl)amino)methyl)-5-methylhexanoic acid

: 925237-15-6
3-(tert-butoxycarbonylamino-methyl)-5-methyl-hexanoic acid 3-{[1-(tert-butoxycarbonylamino-methyl)-cyclohexyl]-acetoxy}-2,2-dimethyl-propyl ester

Guidance literature:: [1-(tert-butoxycarbonylamino-methyl)-cyclohexyl]-acetic acid 3-hydroxy-2,2-dimethyl-propyl ester; (S)-3-(((tert-butoxycarbonyl)amino)methyl)-5-methylhexanoic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 1h; cooling;

With dmap; In dichloromethane; at 20 ℃;
DOI:10.1002/ardp.200400958

Reference yield:

: 227626-60-0
N-Boc-gabapentin

: 925237-15-6
3-(tert-butoxycarbonylamino-methyl)-5-methyl-hexanoic acid 3-{[1-(tert-butoxycarbonylamino-methyl)-cyclohexyl]-acetoxy}-2,2-dimethyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexylcarbodiimide / CH₂Cl₂ / 1 h / cooling

1.2: 4-dimethylaminopyridine / CH₂Cl₂ / 20 °C

2.1: dicyclohexylcarbodiimide / CH₂Cl₂ / 1 h / cooling

2.2: 4-dimethylaminopyridine / CH₂Cl₂ / 20 °C

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/ardp.200400958

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 925237-15-6
3-(tert-butoxycarbonylamino-methyl)-5-methyl-hexanoic acid 3-{[1-(tert-butoxycarbonylamino-methyl)-cyclohexyl]-acetoxy}-2,2-dimethyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexylcarbodiimide / CH₂Cl₂ / 1 h / cooling

1.2: 4-dimethylaminopyridine / CH₂Cl₂ / 20 °C

2.1: dicyclohexylcarbodiimide / CH₂Cl₂ / 1 h / cooling

2.2: 4-dimethylaminopyridine / CH₂Cl₂ / 20 °C

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/ardp.200400958