Propanedioic acid, chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:Propanedioic acid, chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester
CAS No.:92615-17-3
Molecular Formula:C₃₈H₄₁Cl₄NO₈SSi
Molecular Weight:841.709
Hs Code.:

Propanedioic acid,
chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl
methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester

Synonyms:

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Chemical Property of Propanedioic acid, chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester

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Technology Process of Propanedioic acid, chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester

There total 4 articles about Propanedioic acid, chloro[2-oxo-3-[1-[[(2,2,2-trichloroethoxy)carbonyl]oxy]ethyl]-4-[(triphenyl methyl)thio]-1-azetidinyl]-, 2-propenyl 2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92615-19-5
Allyl-trimethylsilylethylketomalonate

: 92615-17-3
2-Chloro-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran

2: SOCl₂, pyridine / CH₂Cl₂

With pyridine; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)88129-0

Reference yield:

: 90744-47-1
2-Oxo-malonic acid bis-(2-trimethylsilanyl-ethyl) ester

: 92615-17-3
2-Chloro-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / K₂CO₃

2: triethylamine / tetrahydrofuran

3: SOCl₂, pyridine / CH₂Cl₂

With pyridine; thionyl chloride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)88129-0

Reference yield:

: 87605-43-4
(3S,4R)-3-[1-(2,2,2)-trichloroethoxycarbonyloxyethyl]-4-(triphenylmethylthio)-azetidin-2-one

: 92615-17-3
2-Chloro-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran

2: SOCl₂, pyridine / CH₂Cl₂

With pyridine; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)88129-0