2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

Base Information

Chemical Name:2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester
CAS No.:87605-53-6
Molecular Formula:C₃₈H₄₂Cl₃NO₉SSi
Molecular Weight:823.263
Hs Code.:

2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

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Chemical Property of 2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

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Technology Process of 2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

There total 2 articles about 2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90744-47-1
2-Oxo-malonic acid bis-(2-trimethylsilanyl-ethyl) ester

: 87605-53-6,87678-73-7,92693-54-4
2-Hydroxy-2-{(3S,4R)-2-oxo-3-[1-(2,2,2-trichloro-ethoxycarbonyloxy)-ethyl]-4-tritylsulfanyl-azetidin-1-yl}-malonic acid allyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / K₂CO₃

2: triethylamine / tetrahydrofuran

With potassium carbonate; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)88129-0