Furan, 3-[4,8-dimethyl-1-[(4-methylphenyl)sulfonyl]-3,7-nonadienyl]-, (E)-

Base Information

Chemical Name:Furan, 3-[4,8-dimethyl-1-[(4-methylphenyl)sulfonyl]-3,7-nonadienyl]-, (E)-
CAS No.:92631-11-3
Molecular Formula:C₂₂H₂₈O₃S
Molecular Weight:372.529
Hs Code.:

Synonyms:

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Chemical Property of Furan, 3-[4,8-dimethyl-1-[(4-methylphenyl)sulfonyl]-3,7-nonadienyl]-, (E)-

Chemical Property:

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Technology Process of Furan, 3-[4,8-dimethyl-1-[(4-methylphenyl)sulfonyl]-3,7-nonadienyl]-, (E)-

There total 1 articles about Furan, 3-[4,8-dimethyl-1-[(4-methylphenyl)sulfonyl]-3,7-nonadienyl]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 92631-12-4
3-(tosylmethyl)furan

: 92631-11-3
1-(3-furyl)-4,8-dimethyl-1-p-tosylnona-3(E),7-diene

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) HMPA, THF, -78 deg C, 20 min, 2.) -78 deg C -> room temperature, 2 h;

Reference yield:

: 92631-11-3
1-(3-furyl)-4,8-dimethyl-1-p-tosylnona-3(E),7-diene

: 92631-17-9
9-p-tosylneotorreyol

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 0.17 h / 0 °C

2: Et₃N / dimethylformamide / 20 h / 60 °C

3: 30percent H₂O₂, AcOH / 20 h / 20 °C

4: trimethyl phosphine, MeOH / 48 h / 20 °C

With methanol; dihydrogen peroxide; acetic acid; triethylamine; trimethylphosphane; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 92631-11-3
1-(3-furyl)-4,8-dimethyl-1-p-tosylnona-3(E),7-diene

: 92631-25-9
6-hydroxy-1-p-tosyldendrolasin

Guidance literature:: Multi-step reaction with 6 steps

1: CH₂Cl₂ / 0.17 h / 0 °C

2: 78 percent / AcOH / 1 h / 20 °C

3: 30percent H₂O₂, AcOH / 20 h / 20 °C

4: NaHCO₃ / toluene / 1.5 h / Heating

5: 77 percent / AcOH, toluene-p-sulphonic acid / diethyl ether; H₂O / 1 h / 0 °C

6: 95 percent / 10percent KOH / ethanol; H₂O / 3 h / 20 °C

With potassium hydroxide; dihydrogen peroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; In diethyl ether; ethanol; dichloromethane; water; toluene;