Technology Process of 2,6-Nonadien-4-ol,
9-(3-furanyl)-2,6-dimethyl-9-[(4-methylphenyl)sulfonyl]-
There total 8 articles about 2,6-Nonadien-4-ol,
9-(3-furanyl)-2,6-dimethyl-9-[(4-methylphenyl)sulfonyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; water;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) n-BuLi / 1.) HMPA, THF, -78 deg C, 20 min, 2.) -78 deg C -> room temperature, 2 h
2: CH2Cl2 / 0.17 h / 0 °C
3: 78 percent / AcOH / 1 h / 20 °C
4: 30percent H2O2, AcOH / 20 h / 20 °C
5: NaHCO3 / toluene / 1.5 h / Heating
6: 77 percent / AcOH, toluene-p-sulphonic acid / diethyl ether; H2O / 1 h / 0 °C
7: 95 percent / 10percent KOH / ethanol; H2O / 3 h / 20 °C
With
potassium hydroxide; n-butyllithium; dihydrogen peroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid;
In
diethyl ether; ethanol; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) n-BuLi / 1.) HMPA, THF, -78 deg C, 20 min, 2.) -78 deg C -> room temperature, 2 h
2: CH2Cl2 / 0.17 h / 0 °C
3: 78 percent / AcOH / 1 h / 20 °C
4: 30percent H2O2, AcOH / 20 h / 20 °C
5: NaHCO3 / toluene / 1.5 h / Heating
6: 77 percent / AcOH, toluene-p-sulphonic acid / diethyl ether; H2O / 1 h / 0 °C
7: 95 percent / 10percent KOH / ethanol; H2O / 3 h / 20 °C
With
potassium hydroxide; n-butyllithium; dihydrogen peroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid;
In
diethyl ether; ethanol; dichloromethane; water; toluene;