Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane

Base Information

Chemical Name:Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane
CAS No.:92682-66-1
Molecular Formula:C₃₁H₂₇ClGe
Molecular Weight:507.598
Hs Code.:
DSSTox Substance ID:DTXSID40534339

Synonyms:92682-66-1;DTXSID40534339;Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane

Suppliers and Price of Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:508.1013063
Heavy Atom Count:33
Complexity:666

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Ge](C)(C1C(=C(C(=C1C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4)C5=CC=CC=C5)Cl

Technology Process of Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane

There total 1 articles about Chloro(dimethyl)(2,3,4,5-tetraphenylcyclopenta-2,4-dien-1-yl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 58081-02-0
tetraphenylcyclopentadienyllithium

: 1529-48-2
dichlorodimethylgermanium

: 92682-66-1
tetraphenylcyclopentadienyldimethylgermane chloride

Guidance literature:: In benzene; refluxing for 3 h;; solvent removed in vac., washed with cold hexane; dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(84)85092-5

Reference yield: 47.0%

: 92682-66-1
tetraphenylcyclopentadienyldimethylgermane chloride

: 16666-80-1
triphenylphosphonio-1-methylethanide

: {(C₆H₅)3PCH(CH₃)2}⁽¹⁺⁾*{(C₆H₅)4C₅Ge(CH₃)2Cl}^(1-) = {(C₆H₅)3PCH(CH₃)2}{(C₆H₅)4C₅Ge(CH₃)2Cl}

Guidance literature:: In tetrahydrofuran; stirred for about day at room temp.; solvent was removed in vac.; benzene was condensed onto residue in vac., and the upper layer was decanted; after removing the benzene from the lower layer and washing the residue with hexane; elem. anal.;
DOI:10.1016/0022-328X(84)85092-5