Benzenepropanamide, a-amino-N-cyclohexyl-

Base Information

• Chemical Name: Benzenepropanamide, a-amino-N-cyclohexyl-
• CAS No.: 92698-80-1
• Molecular Formula: C₁₅H₂₂N₂O
• Molecular Weight: 246.352

Synonyms:2-AMINO-N-CYCLOHEXYL-3-PHENYLPROPANAMIDE;2-Amino-N-cyclohexyl-3-phenylpropionamide;Hydrocinnamamide, α-amino-N-cyclohexyl-;

Chemical Property of Benzenepropanamide, a-amino-N-cyclohexyl-

Chemical Property:

• Boiling Point: 455.7±34.0 °C (760 mmHg)
• PSA: 55.12000
• Density: 1.07±0.1 g/cm3 (20 °C, 760 mmHg)
• LogP: 3.09650

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-N-cyclohexyl-3-phenyl-DL-propanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenepropanamide, a-amino-N-cyclohexyl-

There total 18 articles about Benzenepropanamide, a-amino-N-cyclohexyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

N-tert-butyloxycarbonyl-(L)-phenylalanine cyclohexylamide (169566-77-2) → L-phenylalanine cyclohexylamide (17186-53-7,92698-80-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1002/hlca.19950780305

Reference yield: 82.0%

N-<(S)-1-<(S)-1-cyclohexylcarbamoyl-2-phenyl-ethyl>-3-isobutyl-2,5-dioxo-pyrrolidin-3-yl>-benzamide → L-phenylalanine cyclohexylamide (17186-53-7,92698-80-1) + (S)-N-(1-amino-3-isobutyl-2,5-dioxo-pyrrolidin-3-yl)-benzamide

Guidance literature:

With hydrazine hydrate; In ethanol; for 18h; Heating;

DOI:10.1016/0040-4020(95)00665-U

Reference yield: 81.0%

N-<(R)-1-<(S)-1-cyclohexylcarbamoyl-2-phenyl-ethyl>-3-methyl-2,5-dioxo-pyrrolidin-3-yl>-benzamide → L-phenylalanine cyclohexylamide (17186-53-7,92698-80-1) + (R)-N-(1-amino-3-methyl-2,5-dioxo-pyrrolidin-3-yl)-benzamide

Guidance literature:

With hydrazine hydrate; In ethanol; for 18h; Heating;

DOI:10.1016/0040-4020(95)00665-U

upstream raw materials:

Cbz-L-Phe-cyclohexylNH

acetic acid

N-tert-butyloxycarbonyl-(L)-phenylalanine cyclohexylamide

N-benzyloxycarbonyl-L-phenylalanine p-nitrophenyl ester

Downstream raw materials:

N²-<(R)-N²-benzoyl-2-methyl-phenylalanyl>-(S)-phenylalanine cyclohexylamide

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