MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-

Base Information

Chemical Name:MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-
CAS No.:27389-83-9
Molecular Formula:C17H12 N2 O
Molecular Weight:260.295
Hs Code.:
DSSTox Substance ID:DTXSID10181814
Nikkaji Number:J41.615K

Synonyms:BRN 2125672;p-Benzyloxybenzylidenemalononitrile;MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-;27389-83-9;2-(4-BENZYLOXY-BENZYLIDENE)-MALONONITRILE;Malononitrile, [p-(benzyloxy)benzylidene]-;Oprea1_046290;Oprea1_160279;2-{[4-(benzyloxy)phenyl]methylidene}propanedinitrile;SCHEMBL8167160;DTXSID10181814;GBQGNEMSQIQFRK-UHFFFAOYSA-N;4-(Benzyloxy)benzylidenemalononitrile;MCK100179;AKOS001111839;2-(4-benzyloxybenzylidene)-malononitrile;LS-88855;2-[4-(benzyloxy)benzylidene]malononitrile;Z26177990

Suppliers and Price of MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-

Chemical Property:

Vapor Pressure:1.49E-08mmHg at 25°C
Boiling Point:457.4°Cat760mmHg
Flash Point:183.4°C
Density:1.192g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:260.094963011
Heavy Atom Count:20
Complexity:404

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=CC=C(C=C2)C=C(C#N)C#N

Technology Process of MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)-

There total 4 articles about MALONONITRILE, (p-(BENZYLOXY)BENZYLIDENE)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 4397-53-9
p-benzyloxybenzaldehyde

: 109-77-3
malononitrile

: 27389-83-9
2-(4-benzyloxybenzylidene)-malononitrile

Guidance literature:: With 3-(1-piperazino)propyl functionalised silica gel; In acetonitrile;
DOI:10.1016/j.tet.2005.08.076

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 27389-83-9
2-(4-benzyloxybenzylidene)-malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 100 °C

2: piperidine / ethanol / 24 h / 20 °C

With piperidine; potassium carbonate; potassium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1134/S1070363217030173

Reference yield:

: 100-44-7
benzyl chloride

: 27389-83-9
2-(4-benzyloxybenzylidene)-malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 100 °C

2: piperidine / ethanol / 24 h / 20 °C

With piperidine; potassium carbonate; potassium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1134/S1070363217030173