5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione

Base Information

Chemical Name:5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione
CAS No.:329762-17-6
Molecular Formula:C23H15ClN2O3
Molecular Weight:402.8298
Hs Code.:
DSSTox Substance ID:DTXSID90382983

Synonyms:5-[chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione;DTXSID90382983;5-(chloro(phenyl)methylene)-1,3-diphenylpyrimidine-2,4,6(1H,3H,5H)-trione;329762-17-6

Suppliers and Price of 5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione

Chemical Property:

Vapor Pressure:3.75E-11mmHg at 25°C
Boiling Point:525.9°Cat760mmHg
Flash Point:271.9°C
Density:1.394g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:402.0771200
Heavy Atom Count:29
Complexity:644

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=C2C(=O)N(C(=O)N(C2=O)C3=CC=CC=C3)C4=CC=CC=C4)Cl

Technology Process of 5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione

There total 3 articles about 5-[Chloro(phenyl)methylidene]-1,3-diphenylhexahydropyrimidine-2,4,6-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 182955-13-1
5-Benzoyl-1,3-diphenyl-pyrimidine-2,4,6-trione

: 329762-17-6
5-(Chloro-phenyl-methylene)-1,3-diphenyl-pyrimidine-2,4,6-trione

Guidance literature:: With phosphorus pentachloride; In toluene; for 8h; Heating;
DOI:10.1002/jhet.5570330404

Reference yield:

: 7391-60-8
1,3-diphenylbarbituric acid

: 329762-17-6
5-(Chloro-phenyl-methylene)-1,3-diphenyl-pyrimidine-2,4,6-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 0.5N aq. NaOH / 2.) THF, 20 deg C, 12 h

2: 75 percent / PCl₅ / toluene / 8 h / Heating

With sodium hydroxide; phosphorus pentachloride; In toluene;
DOI:10.1002/jhet.5570330404

Reference yield:

: 98-88-4
benzoyl chloride

: 329762-17-6
5-(Chloro-phenyl-methylene)-1,3-diphenyl-pyrimidine-2,4,6-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 0.5N aq. NaOH / 2.) THF, 20 deg C, 12 h

2: 75 percent / PCl₅ / toluene / 8 h / Heating

With sodium hydroxide; phosphorus pentachloride; In toluene;
DOI:10.1002/jhet.5570330404