3-Methyl-2-(octa-1,7-diynyl)pyridine

Base Information

Chemical Name:3-Methyl-2-(octa-1,7-diynyl)pyridine
CAS No.:927434-21-7
Molecular Formula:C14H15N
Molecular Weight:197.27600
Hs Code.:
DSSTox Substance ID:DTXSID601270979
Mol file:927434-21-7.mol

Synonyms:3-Methyl-2-(octa-1,7-diynyl)pyridine;927434-21-7;DTXSID601270979;Pyridine, 3-methyl-2-(1,7-octadiyn-1-yl)-

Suppliers and Price of 3-Methyl-2-(octa-1,7-diynyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Methyl-2-(octa-1,7-diynyl)pyridine

Chemical Property:

PSA：12.89000
LogP:2.93510
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:197.120449483
Heavy Atom Count:15
Complexity:282

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N=CC=C1)C#CCCCCC#C

Technology Process of 3-Methyl-2-(octa-1,7-diynyl)pyridine

There total 1 articles about 3-Methyl-2-(octa-1,7-diynyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3430-17-9
2-bromo-3-picoline

: 871-84-1
1,7-Octadiyne

: 927434-21-7
3-methyl-2-(octa-1,7-diynyl)pyridine

Guidance literature:: With copper(l) iodide; diisopropylamine; triphenylphosphine; dichloro bis(acetonitrile) palladium(II); In tetrahydrofuran; at 50 ℃;
DOI:10.1016/j.tetasy.2006.11.025

Reference yield: 86.0%

: 927434-21-7
3-methyl-2-(octa-1,7-diynyl)pyridine

: 100-47-0
benzonitrile

: 927434-26-2
5,6,7,8-tetrahydro-1-(3-methylpyridin-2-yl)-3-phenylisoquinoline

Guidance literature:: dicarbonylcyclopentadienylcobalt; at 200 ℃; for 0.333333h; under 3750.3 Torr; microwave irradiation;
DOI:10.1016/j.tetasy.2006.11.025

Reference yield:

: 927434-21-7
3-methyl-2-(octa-1,7-diynyl)pyridine

: 927434-31-9,927814-21-9,927814-23-1
5,6,7,8-tetrahydro-1-(3-methylpyridin-2-yl)-3-phenylisoquinoline N,N'-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / CpCo(CO)2 / 0.33 h / 200 °C / 3750.3 Torr / microwave irradiation

2: 25 percent / m-CPBA / CH₂Cl₂ / 1 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; dicarbonylcyclopentadienylcobalt; In dichloromethane;
DOI:10.1016/j.tetasy.2006.11.025