1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene

Base Information

Chemical Name:1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene
CAS No.:927833-58-7
Molecular Formula:C13H16
Molecular Weight:172.26600
Hs Code.:
DSSTox Substance ID:DTXSID501245335
Nikkaji Number:J2.414.295G
Mol file:927833-58-7.mol

Synonyms:1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene;927833-58-7;MFCD10699574;1-Methyl-4-(1-methyl-3-cyclopenten-1-yl)benzene;Benzene, 1-methyl-4-(1-methyl-3-cyclopenten-1-yl)-;DTXSID501245335;CMB83358;AKOS006305816;AS-68533;SY124621;CS-0038623;W11127

Suppliers and Price of 1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-methyl-4-(1-methylcyclopent-3-en-1-yl)benzene
100mg
$ 310.00

Crysdot
1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene 95+%
5g
$ 2232.00

Crysdot
1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene 95+%
1g
$ 743.00

Chemenu
1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene 95%
1g
$ 701.00

AK Scientific
1-methyl-4-(1-methylcyclopent-3-en-1-yl)benzene
100mg
$ 278.00

Total 2 raw suppliers

Chemical Property of 1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene

Chemical Property:

PSA：0.00000
LogP:3.60270
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:172.125200510
Heavy Atom Count:13
Complexity:186

Purity/Quality:

99% ^*data from raw suppliers

1-methyl-4-(1-methylcyclopent-3-en-1-yl)benzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2(CC=CC2)C

Technology Process of 1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene

There total 7 articles about 1-Methyl-4-(1-methylcyclopent-3-en-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 927833-56-5
4-methyl-4-(4-methylphenyl)-hepta-1,6-diene

: 927833-58-7
1-methyl-4-(1-methylcyclopent-3-enyl)benzene

Guidance literature:: With Grubbs catalyst first generation; In benzene; for 3h; Reflux;
DOI:10.1080/00397911.2010.494812

Reference yield:

: 122-00-9
para-methylacetophenone

: 927833-58-7
1-methyl-4-(1-methylcyclopent-3-enyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / TMSCl; InCl₃ / 1,2-dichloro-ethane / 8 h / 20 °C

2: 90 percent / Grubbs' 1 st generation catalyst / CH₂Cl₂ / 5 h / 20 °C

With indium(III) chloride; chloro-trimethyl-silane; Grubbs' 1 st generation catalyst; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2006.12.023

Reference yield:

: 1310492-49-9
(2-methyl-2-(p-tolyl)cyclopropyl)methyl bromide

: 927833-58-7
1-methyl-4-(1-methylcyclopent-3-enyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile) / benzene / 12 h / Inert atmosphere; Reflux

2: Grubbs catalyst first generation / benzene / 3 h / Reflux

With Grubbs catalyst first generation; 2,2'-azobis(isobutyronitrile); In benzene;
DOI:10.1080/00397911.2010.494812