Benzenamine, N-methyl-N-(trichloroethenyl)-

Base Information

• Chemical Name: Benzenamine, N-methyl-N-(trichloroethenyl)-
• CAS No.: 708-88-3
• Molecular Formula: C9H8Cl3N
• Molecular Weight: 236.528
• DSSTox Substance ID: DTXSID30221064
• Mol file: 708-88-3.mol

Synonyms:Benzenamine, N-methyl-N-(trichloroethenyl)-;N-Methyl-N-(trichloroethenyl)benzenamine;708-88-3;C9H8Cl3N;C9-H8-Cl3-N;DTXSID30221064

Chemical Property of Benzenamine, N-methyl-N-(trichloroethenyl)-

Chemical Property:

• Vapor Pressure: 0.0207mmHg at 25°C
• Boiling Point: 251.3°Cat760mmHg
• Flash Point: 105.8°C
• Density: 1.38g/cm³
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 234.972232
• Heavy Atom Count: 13
• Complexity: 193

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C1=CC=CC=C1)C(=C(Cl)Cl)Cl

Technology Process of Benzenamine, N-methyl-N-(trichloroethenyl)-

There total 4 articles about Benzenamine, N-methyl-N-(trichloroethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methyl-N-phenyltrichloroacetamide (36558-96-0) → N-methyl-N-(trichlorovinyl)aniline (708-88-3)

Guidance literature:

With triphenylphosphine; In benzene;

DOI:10.1021/ja00869a021

Reference yield:

N-methyl-2-chloroacetanilide (2620-05-5) → N-methyl-N-(trichlorovinyl)aniline (708-88-3)

Guidance literature:

With phosphorus pentachloride; In benzene;

DOI:10.1021/jo01059a054

Reference yield:

phenyltrichloromethylmercury (3294-57-3) + N-methylaniline (100-61-8) → N-methyl-N-(trichlorovinyl)aniline (708-88-3)

Guidance literature:

In benzene;

DOI:10.1016/S0040-4039(00)70259-0

upstream raw materials:

N-methyl-N-phenyltrichloroacetamide

phenyltrichloromethylmercury

N-methylaniline

N-methyl-2-chloroacetanilide

Downstream raw materials:

-methyl-phenyl-amin

N-Methyl-N-<(trimethylsilyl)ethinyl>anilin

N-Methyl-N-(triphenylsilylethinyl)anilin

N-methyl N-phenylamino acetylene