2,4-dichloro-N,N-diethylbenzamide

Base Information

• Chemical Name: 2,4-dichloro-N,N-diethylbenzamide
• CAS No.: 24309-78-2
• Molecular Formula: C11H13 Cl2 N O
• Molecular Weight: 246.136
• Mol file: 24309-78-2.mol

Synonyms:N,N-Diethyl-2,4-dichlorobenzamide;NSC 405063

Chemical Property of 2,4-dichloro-N,N-diethylbenzamide

Chemical Property:

• Vapor Pressure: 1.12E-05mmHg at 25°C
• Boiling Point: 370.3°Cat760mmHg
• Flash Point: 177.8°C
• Density: 1.22g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dichloro-N,N-diethylbenzamide

There total 4 articles about 2,4-dichloro-N,N-diethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,4-dichlorobenzotrichloride (13014-18-1) + triethylamine (121-44-8) → 2,4-dichloro-N,N-diethylbenzamide (24309-78-2)

Guidance literature:

With B₁₂ complex immobilized on rhodium(III) modified anatase TiO₂; air; In acetonitrile; at 20 ℃; for 3h; Irradiation;

DOI:10.1016/j.jorganchem.2019.121058

Reference yield: 96.7%

diethylamine (109-89-7) + 2,4-dichlorobenzoyl chloride (89-75-8) → 2,4-dichloro-N,N-diethylbenzamide (24309-78-2)

Guidance literature:

In Isopropyl acetate; toluene; at 20 ℃; for 72h;

DOI:10.1021/op800210x

Reference yield:

2,4-dichlorobenzotrichloride (13014-18-1) + diethylamine (109-89-7) → 2,4-dichloro-N,N-diethylbenzamide (24309-78-2)

Guidance literature:

With heptamethyl Coβ-perchlorato-cob(II)yrinate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 3h; Irradiation;

DOI:10.1002/cplu.201800522

upstream raw materials:

diethylamine

2,4-dichlorobenzoyl chloride

2,4-dichlorobenzotrichloride

triethylamine

Downstream raw materials:

2-chloro-N,N-diethyl-4-propylbenzamide