4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde

Base Information

Chemical Name:4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde
CAS No.:928258-01-9
Molecular Formula:C₁₆H₁₆N₂O₂
Molecular Weight:268.315
Hs Code.:
DSSTox Substance ID:DTXSID80582859

Synonyms:928258-01-9;DTXSID80582859;4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde

Suppliers and Price of 4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:268.121177757
Heavy Atom Count:20
Complexity:325

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1OC)C)N=NC2=CC=C(C=C2)C=O

Technology Process of 4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde

There total 3 articles about 4-[(E)-(4-Methoxy-3,5-dimethylphenyl)diazenyl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928258-00-8
4-(4-hydroxy-3,5-dimethyl-phenylazo)-benzaldehyde

: 74-88-4
methyl iodide

: 928258-01-9
4-(4-methoxy-3,5-dimethyl-phenylazo)-benzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1002/ejoc.200600719

Reference yield:

: 556-18-3,28107-09-7
4-aminobenzaldehyde

: 928258-01-9
4-(4-methoxy-3,5-dimethyl-phenylazo)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. HCl; NaNO₂ / acetone / 0.25 h / -15 °C

1.2: aq. NaOH / acetone / 0.5 h / -15 - 20 °C

2.1: K₂CO₃ / dimethylformamide / 24 h / 20 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/ejoc.200600719

Reference yield:

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 928258-01-9
4-(4-methoxy-3,5-dimethyl-phenylazo)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. HCl; NaNO₂ / acetone / 0.25 h / -15 °C

1.2: aq. NaOH / acetone / 0.5 h / -15 - 20 °C

2.1: K₂CO₃ / dimethylformamide / 24 h / 20 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/ejoc.200600719