(5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name)

Base Information

Chemical Name:(5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name)
CAS No.:528-81-4
Molecular Formula:C6H8O5
Molecular Weight:160.1247
Hs Code.:

Synonyms:6-Deoxy-L-ascorbic acid;L-Ascorbic acid, 6-deoxy-;6-Desoxy-L-ascorbic acid;Ascorbic acid, 6-deoxy-, L-;

Suppliers and Price of (5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name)

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Refractive Index:1.649
Boiling Point:417.573 °C at 760 mmHg
Flash Point:183.221 °C
Density:1.728 g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name)

There total 10 articles about (5R)-3,4-dihydroxy-5-[(1S)-1-hydroxyethyl]furan-2(5H)-one (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 62983-44-2
6-bromo-6-deoxy-(S)-ascorbic acid

: 528-81-4,773041-39-7
6-deoxy-L-ascorbic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; triethylamine; for 5h;
DOI:10.1002/hlca.19800630642

Reference yield:

: 6-bromo-L-ascorbic acid

: 528-81-4,773041-39-7
6-deoxy-L-ascorbic acid

Guidance literature:: With sodium carbonate; palladium-carbon; In water; hydrogen;

Reference yield:

: 18467-77-1
dikegulac

: 528-81-4,773041-39-7
6-deoxy-L-ascorbic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

2: 13 g / Cu(Ac)2 / H₂O / 0.08 h

3: 19.2 g / Br₂, PPh₃ / various solvent(s) / 0.25 h / 80 °C

4: Amberlite JR 120 (H+-form), H₂O / 4 h / Heating

5: 88 percent / H₂ / 5percent Pd/C / methanol; triethylamine / 5 h

With Amberlite JR 120 (H+-form); water; hydrogen; bromine; copper diacetate; potassium carbonate; triphenylphosphine; palladium on activated charcoal; In methanol; water; triethylamine; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19800630642