Technology Process of 2-Penten-1-ol, 5-[4-(1-methylethyl)phenyl]-, methanesulfonate, (E)-
There total 3 articles about 2-Penten-1-ol, 5-[4-(1-methylethyl)phenyl]-, methanesulfonate, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at -5 ℃;
for 0.666667h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) THF, 20 deg C, 2.) 10 deg C, then room temp., 6 h, then 50-55 deg C, 4 h
2: 70 percent / lithium aluminium monoethoxy hydride / diethyl ether
3: 81 percent / NEt3 / CH2Cl2 / 0.67 h / -5 °C
With
lithium monoethoxyaluminum hydride; sodium hydride; triethylamine;
In
diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / lithium aluminium monoethoxy hydride / diethyl ether
2: 81 percent / NEt3 / CH2Cl2 / 0.67 h / -5 °C
With
lithium monoethoxyaluminum hydride; triethylamine;
In
diethyl ether; dichloromethane;