AcetaMide, 2,2,2-trifluoro-N-[4-(trifluoroMethyl)phenyl]-

Base Information

• Chemical Name: AcetaMide, 2,2,2-trifluoro-N-[4-(trifluoroMethyl)phenyl]-
• CAS No.: 67319-83-9
• Molecular Formula: C9H5F6NO
• Molecular Weight: 257.135

Synonyms:4'-(Trifluoromethyl)-2,2,2-trifluoroacetanilide;Phenylamine,N-TFA-4-trifluoromethyl;Acetanilide,2,2,2-trifluoro-4'-(trifluoromethyl);Acetamide,2,2,2-trifluoro-N-(4-(trifluoromethyl)phenyl);

Chemical Property of AcetaMide, 2,2,2-trifluoro-N-[4-(trifluoroMethyl)phenyl]-

Chemical Property:

• Vapor Pressure: 0.0227mmHg at 25°C
• Boiling Point: 249.6°Cat760mmHg
• Flash Point: 104.8°C
• PSA: 29.10000
• Density: 1.491g/cm³
• LogP: 3.27920

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AcetaMide, 2,2,2-trifluoro-N-[4-(trifluoroMethyl)phenyl]-

There total 7 articles about AcetaMide, 2,2,2-trifluoro-N-[4-(trifluoroMethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-trifluoromethylphenylamine (455-14-1) + trifluoroacetic acid (76-05-1) → 2,2,2-trifluoro-N-(4-(trifluoromethyl)phenyl)acetamide (67319-83-9)

Guidance literature:

With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; at 20 ℃; for 0.25h;

DOI:10.2174/157017811797249317

Reference yield: 77.0%

C20H13F3NOS2(1+)*BF4(1-) + trifluoromethylcopper(I) (77152-08-0) → 2,2,2-trifluoro-N-(4-(trifluoromethyl)phenyl)acetamide (67319-83-9)

Guidance literature:

With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; In acetonitrile; at 30 ℃; for 3h; Sealed tube; Irradiation;

DOI:10.1002/anie.201906672

Reference yield: 63.0%

4-trifluoromethylphenylamine (455-14-1) + trifluoroacetic anhydride (407-25-0) → 2,2,2-trifluoro-N-(4-(trifluoromethyl)phenyl)acetamide (67319-83-9)

Guidance literature:

In N,N-dimethyl-formamide; for 48h; Ambient temperature;

upstream raw materials:

4-trifluoromethylphenylamine

trifluoroacetic anhydride

trifluoroacetic acid

2,2,2-trifluoro-N-(4-iodophenyl)acetamide

Downstream raw materials:

2,2,2-trifluoro-N-trideuteriomethyl-N-(4-trifluoromethyl-phenyl)-acetamide

4-hydroxy-5-methoxy-N-trideuteriomethyl-1-methyl-2-oxo-N-[(4-trifluoromethyl)phenyl]-1,2-dihydroquinoline-3-carboxamide

4-trifluoromethyl-2-nitroaniline

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