1,4,7,10,13-Pentathiacyclopentadecane

Base Information

• Chemical Name: 1,4,7,10,13-Pentathiacyclopentadecane
• CAS No.: 36338-04-2
• Molecular Formula: C10H20 S5
• Molecular Weight: 0
• Hs Code.: 2934999090
• Mol file: 36338-04-2.mol

Synonyms:15-Ethano-S5;15-Thiacrown-5; NSC 650801

Chemical Property of 1,4,7,10,13-Pentathiacyclopentadecane

Chemical Property:

• Vapor Pressure: 8.55E-09mmHg at 25°C
• Boiling Point: 476.8°C at 760 mmHg
• Flash Point: 253.5°C
• PSA: 126.50000
• Density: 1.14g/cm³
• LogP: 3.66600

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4,7,10,13-Pentathiacyclopentadecane

There total 3 articles about 1,4,7,10,13-Pentathiacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thirane (420-12-2) → 1,4,7,10,13,16-hexathiacyclooctadecan (296-41-3) + 1,4,7,10-tetrathiacyclododecane (25423-56-7) + 1,4,7,10,13-pentathiacyclopentadecane (36338-04-2)

Guidance literature:

With dimethyl acetylenedicarboxylate; pentacarbonyl(acetonitrile)tungsten; In various solvent(s); at 25 ℃; for 6h; Further Variations:; Catalysts; Reagents; Product distribution;

DOI:10.1016/S0022-328X(02)01307-4

Reference yield:

3-thiapentan-1,5-dithiol (3570-55-6) + 3,6-dithia-1,8-octanediol bimesylate (95121-77-0) → 1,4,7,10,13-pentathiacyclopentadecane (36338-04-2) + 1,4,7,10,13,16,19,22,25,28-Decathia-cyclotriacontane

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 6h; Yield given;

DOI:10.1021/ja00294a034

Reference yield:

→ 1,4,7,10,13-pentathiacyclopentadecane (36338-04-2)

Guidance literature:

DOI:10.1021/jo00928a023

upstream raw materials:

3-thiapentan-1,5-dithiol

3,6-dithia-1,8-octanediol bimesylate

thirane

Downstream raw materials:

{Ag(C₁₀H₂₀S₅)}⁽¹⁺⁾*{B(C₆F₅)4}^(1-)={Ag(C₁₀H₂₀S₅)}{B(C₆F₅)4}

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