2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride

Base Information

• Chemical Name: 2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride
• CAS No.: 22304-57-0
• Molecular Formula: C9F10 O2
• Molecular Weight: 330.082
• Hs Code.: 2918990090
• European Community (EC) Number: 244-902-4
• DSSTox Substance ID: DTXSID70885200
• Nikkaji Number: J285.479A
• Mol file: 22304-57-0.mol

Synonyms:22304-57-0;2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride;Perfluoro(2-phenoxypropionyl fluoride);EINECS 244-902-4;Propanoyl fluoride, 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)-;Propanoyl fluoride, 2,3,3,3-tetrafluoro-2-(2,3,4,5,6-pentafluorophenoxy)-;SCHEMBL11282885;C9F10O2;DTXSID70885200;C9-F10-O2;perfluoro-2-phenoxypropionyl fluoride;Propionyl fluoride, tetrafluoro-2-(pentafluorophenoxy)-;2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propanoic acid fluoride;2,3,3,3-Tetrafluoro-2-(2,3,4,5,6-pentafluorophenoxy)-propanoyl fluoride

Chemical Property of 2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride

Chemical Property:

• Vapor Pressure: 0.239mmHg at 25°C
• Boiling Point: 206.3°Cat760mmHg
• Flash Point: 76.6°C
• PSA: 26.30000
• Density: 1.719g/cm³
• LogP: 3.48510
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 3
• Exact Mass: 329.97386086
• Heavy Atom Count: 21
• Complexity: 385

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1(=C(C(=C(C(=C1F)F)F)F)F)OC(C(=O)F)(C(F)(F)F)F

Technology Process of 2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride

There total 5 articles about 2,3,3,3-Tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

Hexafluoropropene oxide (428-59-1,25038-02-2) + potassium perfluorophenolate (4615-85-4) → C18F28O5 + 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride (22304-57-0) + 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(pentafluorophenoxy)propoxy]propionyl fluoride (25711-77-7) + 2,3,3,3-Tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(1,1,2,3,3,3-hexafluoro-2-pentafluorophenyloxy-propoxy)-propoxy]-propionyl fluoride (63767-12-4)

Guidance literature:

With 2,2,3,3,4,4,5-heptafluoro-5-nonafluorobutyl-tetrahydro-furan; In 1,2-dimethoxyethane; Tetraethylene glycol dimethyl ether; at 10 - 35 ℃; for 0.666667h; Product distribution / selectivity;

Reference yield:

Hexafluoropropene oxide (428-59-1,25038-02-2) + potassium perfluorophenolate (4615-85-4) → C15F14O3 + 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride (22304-57-0) + 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(pentafluorophenoxy)propoxy]propionyl fluoride (25711-77-7) + 2,3,3,3-Tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(1,1,2,3,3,3-hexafluoro-2-pentafluorophenyloxy-propoxy)-propoxy]-propionyl fluoride (63767-12-4)

Guidance literature:

With 2,2,3,3,4,4,5-heptafluoro-5-nonafluorobutyl-tetrahydro-furan; In 1,2-dimethoxyethane; at -78 - 25 ℃; Product distribution / selectivity;

Reference yield:

Hexafluoropropene oxide (428-59-1,25038-02-2) + potassium perfluorophenolate (4615-85-4) → C15F14O3 + 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride (22304-57-0) + 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(pentafluorophenoxy)propoxy]propionyl fluoride (25711-77-7)

Guidance literature:

In 1,2-dimethoxyethane; Tetraethylene glycol dimethyl ether; at -35 - -10 ℃; for 0.833333 - 0.933333h; Product distribution / selectivity;

upstream raw materials:

Hexafluoropropene oxide

potassium perfluorophenolate

Downstream raw materials:

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(pentafluorophenoxy)propoxy]propionyl fluoride

perfluoro(2-propoxypropionyl) fluoride

perfluoro-2,5-dimethyl-3,6-dioxanonanoyl fluoride

Refernces