Benzene, (2-nitropropyl)-, (S)-

Base Information

Chemical Name:Benzene, (2-nitropropyl)-, (S)-
CAS No.:92998-95-3
Molecular Formula:C9H11NO2
Molecular Weight:165.192
Hs Code.:

Synonyms:

Suppliers and Price of Benzene, (2-nitropropyl)-, (S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (2-nitropropyl)-, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, (2-nitropropyl)-, (S)-

There total 6 articles about Benzene, (2-nitropropyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 705-60-2,18315-84-9,58321-79-2
1-phenyl-2-nitroprop-1-ene

: 92998-95-3
(S)-1-phenyl-2-nitropropane

: 67375-21-7
(R)-1-phenyl-2-nitropropane

: 103-79-7,136675-26-8
1-phenyl-acetone

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; hydrogen; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In dichloromethane; at 50 ℃; for 24h; under 60804.1 Torr; Reagent/catalyst; enantioselective reaction; Autoclave;
DOI:10.1039/c4cc03942d

Reference yield:

: 100-52-7
benzaldehyde

: 92998-95-3
(S)-1-phenyl-2-nitropropane

: 67375-21-7
(R)-1-phenyl-2-nitropropane

: 103-79-7,136675-26-8
1-phenyl-acetone

Guidance literature:: Multi-step reaction with 2 steps

1: N-butylamine; acetic acid / 60 °C / Sonication

2: (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; hydrogen; bis(norbornadiene)rhodium(l)tetrafluoroborate / dichloromethane / 24 h / 50 °C / 60804.1 Torr / Autoclave

With bis(norbornadiene)rhodium(l)tetrafluoroborate; hydrogen; acetic acid; N-butylamine; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In dichloromethane; 1: |Henry Nitro Aldol Condensation;
DOI:10.1039/c4cc03942d

Reference yield:

: 705-60-2,18315-84-9,58321-79-2
1-phenyl-2-nitroprop-1-ene

: 92998-95-3
(S)-1-phenyl-2-nitropropane

: 67375-21-7
(R)-1-phenyl-2-nitropropane

Guidance literature:: With glucose-6-phosphate; pentaerythritol tetranitrate reductase; NADP+; glucose 6-phosphate dehydrogenase; In 2,2,4-trimethylpentane; sec-Butylbenzene; at 30 ℃; for 72h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Inert atmosphere; Enzymatic reaction;
DOI:10.1002/adsc.200800561