N-Benzyl-2-bromo-propionanilide

Base Information

Chemical Name:N-Benzyl-2-bromo-propionanilide
CAS No.:93010-41-4
Molecular Formula:C16H16BrNO
Molecular Weight:318.213
Hs Code.:
Mol file:93010-41-4.mol

Synonyms:N-benzyl-N-phenyl-2-bromopropanamide;N-Benzyl-2-bromo-propionanilide;2-Brom-propionsaeure-(N-benzyl-anilid);N-Benzyl-2-bromo-N-phenylpropionamide;2-Bromo-N-phenyl-N-(phenylmethyl)propanamide;(+-)-2-Brom-propionsaeure-(N-phenyl-benzylamid);2-bromo-propionic acid-(N-benzyl-anilide);

Suppliers and Price of N-Benzyl-2-bromo-propionanilide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-Benzyl-2-bromo-N-phenylpropionamide 97%
5g
$ 83.50

American Custom Chemicals Corporation
N-BENZYL-2-BROMO-N-PHENYLPROPIONAMIDE 95.00%
5G
$ 867.48

AK Scientific
N-Benzyl-2-bromo-N-phenylpropionamide
5g
$ 156.00

Total 3 raw suppliers

Chemical Property of N-Benzyl-2-bromo-propionanilide

Chemical Property:

Melting Point:75-80 °C
PSA：20.31000
LogP:4.00320

Purity/Quality:: N-Benzyl-2-bromo-N-phenylpropionamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Uses N-Benzyl-2-bromo-propionanilide can be used in Ni-pybox catalyzed asymmetric Negishi couplings. Used in Ni-pybox catalyzed asymmetric Negishi couplings.

Technology Process of N-Benzyl-2-bromo-propionanilide

There total 4 articles about N-Benzyl-2-bromo-propionanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 758640-21-0,103-32-2
N-Benzylaniline

: 7148-74-5
2-Bromopropionyl chloride

: 93010-41-4
(±)-N-benzyl-2-bromo-N-phenylpropionamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 3.5h;
DOI:10.1002/anie.202000860

Reference yield:

: 758640-21-0,103-32-2
N-Benzylaniline

: 563-76-8
α-bromopropionyl bromide

: 93010-41-4
(±)-N-benzyl-2-bromo-N-phenylpropionamide

Guidance literature:: With diethyl ether;

Reference yield:

: 62-53-3
aniline

: 93010-41-4
(±)-N-benzyl-2-bromo-N-phenylpropionamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 20 °C

1.2: 0 - 20 °C

2.1: triethylamine / tetrahydrofuran / 3.5 h / 0 - 20 °C

With triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.202000860