3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[[2-[[(cyanoamino)(methylthio)methylene]amino]eth oxy]methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Base Information

• Chemical Name: 3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[[2-[[(cyanoamino)(methylthio)methylene]amino]eth oxy]methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester
• CAS No.: 93117-86-3
• Molecular Formula: C23H27ClN4O5S
• Molecular Weight: 507.01

Synonyms:

Chemical Property of 3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[[2-[[(cyanoamino)(methylthio)methylene]amino]eth oxy]methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[[2-[[(cyanoamino)(methylthio)methylene]amino]eth oxy]methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester

There total 2 articles about 3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[[2-[[(cyanoamino)(methylthio)methylene]amino]eth oxy]methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-42-9) + dimethyl N-cyanodithioiminocarbonate (10191-60-3) → N-<2-<<4-(2-Chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-N'-cyano-S-methylisothiourea (93117-86-3)

Guidance literature:

In isopropyl alcohol; for 4h; Ambient temperature;

DOI:10.1021/jm00123a009

Reference yield:

2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-42-9) + dimethyl N-cyanodithioiminocarbonate (10191-60-3) → N-{2-[(4-{2-Chlorophenyl}-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl)methoxy]ethyl}-N'-cyano-S-methyl-isothiourea (93117-86-3)

Guidance literature:

In isopropyl alcohol;

Reference yield: 79.0%

N-<2-<<4-(2-Chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-N'-cyano-S-methylisothiourea (93117-86-3) + N,N-dimethylethylenediamine (108-00-9) → 1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-2-cyano-3-<2-(dimethylamino)ethyl>guanidine (93848-91-0)

Guidance literature:

at 95 ℃; for 1.5h;

DOI:10.1021/jm00164a019

upstream raw materials:

2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

dimethyl N-cyanodithioiminocarbonate

Downstream raw materials:

2-<<2-<(3-Amino-1H-1,2,4-triazol-5-yl)amino>ethoxy>methyl>-4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine

1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-2-cyano-3-<2-(dimethylamino)ethyl>guanidine

1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-2-cyano-3-methylguanidine

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