3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-hydrochloride salt

Base Information

• Chemical Name: 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-hydrochloride salt
• CAS No.: 93206-04-3
• Molecular Formula: C4H7N5O.ClH
• Molecular Weight: 177.59200
• Mol file: 93206-04-3.mol

Synonyms:1,2,4-Triazin-5(2H)-one, 3-amino-6-(aminomethyl)-, monohydrochloride;

Chemical Property of 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-hydrochloride salt

Chemical Property:

• PSA: 110.68000
• LogP: 0.28930

Purity/Quality:

99% ^*data from raw suppliers

3-Amino-6-(aminomethyl)-1,2,4-triazin-5(2H)-onemonohydrochloride ^*data from reagent suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-hydrochloride salt

There total 1 articles about 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-amino-6-((dibenzylamino)methyl)-1,2,4-triazine-5-(4H)-one (93206-03-2) → 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-one hydrochloride (93206-04-3)

Guidance literature:

With hydrogenchloride; hydrogen; palladium oxide on charcoal; In ethanol; under 760 Torr;

DOI:10.1002/jhet.5570210313

Reference yield: 50.0%

3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-one hydrochloride (93206-04-3) + 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino- and D-ribo-hexonic acid (675124-51-3) → N-<(3-amino-4,5-dihydro-5-oxo-1,2,i4-triazin-6-yl)methyl>-2,5-anhydro-4,6-di-O-benzoyl-D-arabino-and-D-ribo-hexonamide (98748-28-8,98748-29-9)

Guidance literature:

With sodium hydroxide; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In ethanol; water; at 70 ℃; for 3h;

DOI:10.1039/P19850000621

Reference yield: 43.0%

<2-(benzoyloxy)ethoxy>acetic acid (93206-05-4) + 3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-one hydrochloride (93206-04-3) → 2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate (93206-06-5)

Guidance literature:

With sodium hydroxide; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In water; at 70 ℃; for 3h;

DOI:10.1002/jhet.5570210313

upstream raw materials:

3-amino-6-((dibenzylamino)methyl)-1,2,4-triazine-5-(4H)-one

Downstream raw materials:

2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

N-<(3-amino-4,5-dihydro-5-oxo-1,2,i4-triazin-6-yl)methyl>-2,5-anhydro-4,6-di-O-benzoyl-D-arabino-and-D-ribo-hexonamide

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