6-Oxa-2,4-dithia-3-stibaoctanethioic acid, 7-methyl-3-phenyl-5-thioxo-, O-(1-methylethyl) ester

Base Information

Chemical Name:6-Oxa-2,4-dithia-3-stibaoctanethioic acid, 7-methyl-3-phenyl-5-thioxo-, O-(1-methylethyl) ester
CAS No.:93215-78-2
Molecular Formula:C₁₄H₁₉O₂S₄Sb
Molecular Weight:469.318
Hs Code.:

Synonyms:

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Chemical Property of 6-Oxa-2,4-dithia-3-stibaoctanethioic acid, 7-methyl-3-phenyl-5-thioxo-, O-(1-methylethyl) ester

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Technology Process of 6-Oxa-2,4-dithia-3-stibaoctanethioic acid, 7-methyl-3-phenyl-5-thioxo-, O-(1-methylethyl) ester

There total 1 articles about 6-Oxa-2,4-dithia-3-stibaoctanethioic acid, 7-methyl-3-phenyl-5-thioxo-, O-(1-methylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 91208-51-4
phenyldiisopropoxystibine

: 93215-78-2
C₆H₅Sb(S₂COCH(CH₃)2)2

Guidance literature:: In carbon disulfide; refluxing of Sb-compd. (prepared from C6H5SbCl2 and sodium alkoxide) in CS2 for 1 h; removal of solvent under vac.;

Reference yield:

: 93215-78-2
C₆H₅Sb(S₂COCH(CH₃)2)2

: 5035-52-9
dichlorophenylstibine

: C₆H₅^(1-)*Sb⁽³⁺⁾*(CH₃)2CHOCSS^(1-)*Cl^(1-) = C₆H₅Sb(S₂COCH(CH₃)2)Cl

Guidance literature:: In carbon disulfide; equimolar soln. of educts in CS2 stirred for 3 h at room temp.; solvent removed under vac.; elem. anal.;