Technology Process of Benzoic acid, 5-chloro-2-[(2-methylphenyl)thio]-
There total 1 articles about Benzoic acid, 5-chloro-2-[(2-methylphenyl)thio]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; copper;
In
water;
for 11h;
Yield given;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaBH4,BF3.O(C2H5)2 / tetrahydrofuran / 1)mixed at 15 deg C 2)stirred 3h room temp. 3)stand overnight
2: SOCl2 / pyridine / 1)stirred 2h at 20 deg C 2)stand overnight 3)35 - 40 deg C, 1h
With
sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate;
In
tetrahydrofuran; pyridine;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaBH4,BF3.O(C2H5)2 / tetrahydrofuran / 1)mixed at 15 deg C 2)stirred 3h room temp. 3)stand overnight
2: SOCl2 / pyridine / 1)stirred 2h at 20 deg C 2)stand overnight 3)35 - 40 deg C, 1h
3: CHCl3 / 10 h / Heating
With
sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate;
In
tetrahydrofuran; pyridine; chloroform;
