Piperazine, 1-[[5-chloro-2-[(2-methylphenyl)thio]phenyl]methyl]-4-methyl-

Base Information

Chemical Name:Piperazine, 1-[[5-chloro-2-[(2-methylphenyl)thio]phenyl]methyl]-4-methyl-
CAS No.:93289-01-1
Molecular Formula:C₁₉H₂₃ClN₂S
Molecular Weight:346.924
Hs Code.:

Synonyms:

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Chemical Property of Piperazine, 1-[[5-chloro-2-[(2-methylphenyl)thio]phenyl]methyl]-4-methyl-

Chemical Property:

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Technology Process of Piperazine, 1-[[5-chloro-2-[(2-methylphenyl)thio]phenyl]methyl]-4-methyl-

There total 5 articles about Piperazine, 1-[[5-chloro-2-[(2-methylphenyl)thio]phenyl]methyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13421-00-6
5-chloro-2-iodo-benzoic acid

: 93289-01-1
1-<5-chloro-2-(2-methylphenylthio)benzyl>-4-methylpiperazine

Guidance literature:: Multi-step reaction with 4 steps

1: KOH,Cu / H₂O / 11 h / Heating

2: NaBH₄,BF_3.O(C₂H₅)2 / tetrahydrofuran / 1)mixed at 15 deg C 2)stirred 3h room temp. 3)stand overnight

3: SOCl₂ / pyridine / 1)stirred 2h at 20 deg C 2)stand overnight 3)35 - 40 deg C, 1h

4: CHCl₃ / 10 h / Heating

With potassium hydroxide; sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate; copper; In tetrahydrofuran; pyridine; chloroform; water;

Reference yield:

: 93288-99-4
5-chloro-2-(2-methylphenylthio)benzyl alcohol

: 93289-01-1
1-<5-chloro-2-(2-methylphenylthio)benzyl>-4-methylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / pyridine / 1)stirred 2h at 20 deg C 2)stand overnight 3)35 - 40 deg C, 1h

2: CHCl₃ / 10 h / Heating

With thionyl chloride; In pyridine; chloroform;

Reference yield:

: 93288-98-3
5-chloro-2-(2-methylphenylthio)benzoic acid

: 93289-01-1
1-<5-chloro-2-(2-methylphenylthio)benzyl>-4-methylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄,BF_3.O(C₂H₅)2 / tetrahydrofuran / 1)mixed at 15 deg C 2)stirred 3h room temp. 3)stand overnight

2: SOCl₂ / pyridine / 1)stirred 2h at 20 deg C 2)stand overnight 3)35 - 40 deg C, 1h

3: CHCl₃ / 10 h / Heating

With sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate; In tetrahydrofuran; pyridine; chloroform;