6-(Vinyloxy)quinoline

Base Information

• Chemical Name: 6-(Vinyloxy)quinoline
• CAS No.: 59195-18-5
• Molecular Formula: C11H9NO
• Molecular Weight: 171.1953
• DSSTox Substance ID: DTXSID20207933
• Nikkaji Number: J84.936G
• Wikidata: Q83081952

Synonyms:6-(Vinyloxy)quinoline;59195-18-5;Quinoline, 6-(vinyloxy)-;BRN 1525773;6-vinyloxyquinoline;6-Vinyloxy-quinoline;Oprea1_073995;DTXSID20207933;LS-142195

Chemical Property of 6-(Vinyloxy)quinoline

Chemical Property:

• Vapor Pressure: 0.00394mmHg at 25°C
• Boiling Point: 288.9°Cat760mmHg
• Flash Point: 106°C
• Density: 1.123g/cm³
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 171.068413911
• Heavy Atom Count: 13
• Complexity: 181

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=COC1=CC2=C(C=C1)N=CC=C2

Technology Process of 6-(Vinyloxy)quinoline

There total 6 articles about 6-(Vinyloxy)quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

6-hydroxyquinoline (580-16-5) + tetravinyltin (IV) (1112-56-7) → 6-vinyloxyquinoline (59195-18-5)

Guidance literature:

With copper diacetate; oxygen; In acetonitrile; at 20 ℃; for 22h;

DOI:10.1021/jo016037z

Reference yield: 51.0%

6-hydroxyquinoline (580-16-5) + acetylene (74-86-2,25067-58-7) → 6-vinyloxyquinoline (59195-18-5)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; water; at 200 - 210 ℃; for 1h; under 10297.1 - 11768.1 Torr;

DOI:10.1007/BF00758462

Reference yield:

6-(2-chloroethoxy)quinoline hydrochloride → 6-vinyloxyquinoline (59195-18-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 80 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.tetlet.2016.11.061

upstream raw materials:

6-hydroxyquinoline

acetylene

tetravinyltin (IV)

6-bromoquinoline

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