1H-Pyrrole-2-carboxylic acid, 5,5'-[[2,6-bis(acetylamino)phenyl]methylene]bis[3-butyl-4-methyl-, phenylmethyl ester

Base Information

Chemical Name:1H-Pyrrole-2-carboxylic acid, 5,5'-[[2,6-bis(acetylamino)phenyl]methylene]bis[3-butyl-4-methyl-, phenylmethyl ester
CAS No.:93341-89-0
Molecular Formula:C₄₅H₅₂N₄O₆
Molecular Weight:744.931
Hs Code.:

Synonyms:

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Chemical Property of 1H-Pyrrole-2-carboxylic acid, 5,5'-[[2,6-bis(acetylamino)phenyl]methylene]bis[3-butyl-4-methyl-, phenylmethyl ester

Chemical Property:

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Technology Process of 1H-Pyrrole-2-carboxylic acid, 5,5'-[[2,6-bis(acetylamino)phenyl]methylene]bis[3-butyl-4-methyl-, phenylmethyl ester

There total 8 articles about 1H-Pyrrole-2-carboxylic acid, 5,5'-[[2,6-bis(acetylamino)phenyl]methylene]bis[3-butyl-4-methyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 90744-34-6
diacetamido-2,6 benzaldehyde

: 93341-77-6
benzyloxycarbonyl-2 butyl-3 methyl-4 pyrrol

: 93341-89-0
C₄₅H₅₂N₄O₆

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 48h; Heating;

Reference yield:

: 34549-87-6
ethyl 4-butyl-3,5-dimethylpyrrole-2-carboxylate

: 93341-89-0
C₄₅H₅₂N₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1: 67 percent / sodium / 4 h / 80 °C / 15 Torr

2: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

3: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

4: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

5: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

6: 70 percent / sodium / 4 h / 80 °C / 15 Torr

7: 60 percent / paratoluenesulfonic acid / benzene / 48 h / Heating

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; hydrogen; iodine; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; In tetrahydrofuran; ethanol; water; benzene;

Reference yield:

: 1540-36-9
3-butylpentane-2,4-dione

: 93341-89-0
C₄₅H₅₂N₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) zinc, sodium acetate / 1.) acetic acid, 80 deg C, 40 min; 2.) acetic acid, 20 min, 95-105 deg C

2: 67 percent / sodium / 4 h / 80 °C / 15 Torr

3: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

4: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

5: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

6: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

7: 70 percent / sodium / 4 h / 80 °C / 15 Torr

8: 60 percent / paratoluenesulfonic acid / benzene / 48 h / Heating

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; hydrogen; iodine; sodium acetate; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; zinc; In tetrahydrofuran; ethanol; water; benzene;