Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-

Base Information

Chemical Name:Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-
CAS No.:93621-65-9
Molecular Formula:C24H20N2O2
Molecular Weight:368.435
Hs Code.:
NSC Number:167921
DSSTox Substance ID:DTXSID80304876
Nikkaji Number:J1.323.587B
Wikidata:Q82051173

Synonyms:93621-65-9;Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-;NSC167921;SCHEMBL20436327;DTXSID80304876;AQCCBDGMEOKIOL-UHFFFAOYSA-N;NSC-167921;1,1'-Binaphthyl, 2,2'-diacetamido-

Suppliers and Price of Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-

Chemical Property:

PSA：65.18000
LogP:6.87580
XLogP3:4.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:368.152477885
Heavy Atom Count:28
Complexity:527

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=C(C2=CC=CC=C2C=C1)C3=C(C=CC4=CC=CC=C43)NC(=O)C

Technology Process of Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis-

There total 1 articles about Acetamide, N,N'-[1,1'-binaphthalene]-2,2'-diylbis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4488-22-6,18531-95-8
1,1'-binaphthalene-2,2'-diamine

: 75-36-5
acetyl chloride

: 93621-65-9
2,2'-bis(acetamido)-1,1'-binaphthyl

Guidance literature:: With pyridine; In benzene; Ambient temperature;
DOI:10.1246/bcsj.57.2171

Reference yield:

: 93621-65-9
2,2'-bis(acetamido)-1,1'-binaphthyl

: 1229013-43-7,906373-48-6,906373-49-7
(+/-)-3,3'-diphenyl-1,1'-binaphthyl-2,2'-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: silver(I) acetate; palladium diacetate; trifluoroacetic acid / 6 h / Heating

2: sodium hydroxide / ethanol / 44 h / 130 °C

With silver(I) acetate; palladium diacetate; trifluoroacetic acid; sodium hydroxide; In ethanol;
DOI:10.1002/hlca.201700158

Reference yield:

: 93621-65-9
2,2'-bis(acetamido)-1,1'-binaphthyl

: C₃₄H₂₈N₂

Guidance literature:: Multi-step reaction with 4 steps

1: silver(I) acetate; palladium diacetate; trifluoroacetic acid / 6 h / Heating

2: sodium hydroxide / ethanol / 44 h / 130 °C

3: pyridine / dichloromethane / 0 - 20 °C

4: lithium aluminium tetrahydride / 1,4-dioxane / 72 h / Heating

With pyridine; lithium aluminium tetrahydride; silver(I) acetate; palladium diacetate; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1002/hlca.201700158