Butanoic acid, 4-[[1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl]amino]-4-oxo-, (S)-

Base Information

Chemical Name:Butanoic acid, 4-[[1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl]amino]-4-oxo-, (S)-
CAS No.:93627-41-9
Molecular Formula:C14H23NO3
Molecular Weight:253.342
Hs Code.:

Synonyms:

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Chemical Property of Butanoic acid, 4-[[1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl]amino]-4-oxo-, (S)-

Chemical Property:

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Technology Process of Butanoic acid, 4-[[1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl]amino]-4-oxo-, (S)-

There total 4 articles about Butanoic acid, 4-[[1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl]amino]-4-oxo-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108-30-5
succinic acid anhydride

: 67895-57-2
(–)-α-terpinyl amine

: 93627-41-9
(S)-N-(1-p-menthen-8-yl)succinamic acid

Guidance literature:: With triethylamine; In 1,4-dioxane; roomtemp., 20 min then 75 degC 90 min;
DOI:10.1002/hlca.19840670417

Reference yield:

: 10482-56-1,2438-12-2
(-)-(S)-α-terpineol

: 93627-41-9
(S)-N-(1-p-menthen-8-yl)succinamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂ / diethyl ether / 6 h / Ambient temperature

2: HN₃, BF₃*Et₂O / benzene / 2 h / Ambient temperature

3: 71 percent / LiAlH₄ / diethyl ether / 16 h / Heating; resolved with L(+)-tartaric acid

4: 74 percent / Et₃N / dioxane / roomtemp., 20 min then 75 degC 90 min

With lithium aluminium tetrahydride; tris-(2-chloro-ethyl)-amine; boron trifluoride diethyl etherate; bromine; triethylamine; In 1,4-dioxane; diethyl ether; benzene;
DOI:10.1002/hlca.19840670417

Reference yield:

: 2-((1S,3R,4R)-3,4-Dibromo-4-methyl-cyclohexyl)-propan-2-ol

: 93627-41-9
(S)-N-(1-p-menthen-8-yl)succinamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: HN₃, BF₃*Et₂O / benzene / 2 h / Ambient temperature

2: 71 percent / LiAlH₄ / diethyl ether / 16 h / Heating; resolved with L(+)-tartaric acid

3: 74 percent / Et₃N / dioxane / roomtemp., 20 min then 75 degC 90 min

With lithium aluminium tetrahydride; tris-(2-chloro-ethyl)-amine; boron trifluoride diethyl etherate; triethylamine; In 1,4-dioxane; diethyl ether; benzene;
DOI:10.1002/hlca.19840670417