2-Bromo-N,N-diethylethanamine

Base Information

• Chemical Name: 2-Bromo-N,N-diethylethanamine
• CAS No.: 5392-81-4
• Molecular Formula: C6H14BrN
• Molecular Weight: 180.088
• Hs Code.: 2921199090
• NSC Number: 6301
• DSSTox Substance ID: DTXSID00902530
• Nikkaji Number: J342.893A
• Mol file: 5392-81-4.mol

Synonyms:2-Bromo-N,N-diethylethanamine;5392-81-4;Ethanamine, 2-bromo-N,N-diethyl-;(2-bromoethyl)diethylamine;N,N-Diethylaminoethyl bromide hydrobromide;NSC6301;diethylaminoethyl bromide;NoName_3043;2-bromoethyl-diethylamine;N,N-diethylaminoethyl bromide;2-(Diethylamino)ethyl bromide;SCHEMBL397032;2-bromo-N,N-diethylethylamine;N,N-diethyl-2-aminobromoethane;N,N-diethyl-2-amino-bromoethane;(2-bromoethyl)-N,N-diethylamine;DTXSID00902530;2-Bromo-N,N-diethylethanamine #;n-(2-bromoethyl)-n,n-diethylamine;ADAL1134238;NSC-6301;AKOS009159108

Chemical Property of 2-Bromo-N,N-diethylethanamine

Chemical Property:

• Melting Point: 211-215oC (dec.)(lit.)
• Boiling Point: 161.6°Cat760mmHg
• Flash Point: 51.5°C
• PSA: 3.24000
• Density: g/cm³
• LogP: 2.68120
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 179.03096
• Heavy Atom Count: 8
• Complexity: 43.8

Purity/Quality:

99%min ^*data from raw suppliers

2-Bromo-N,N-diethylethylamine hydrobromide 98% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 25-37/38-41
• Safety Statements: 26-39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)CCBr

Technology Process of 2-Bromo-N,N-diethylethanamine

There total 4 articles about 2-Bromo-N,N-diethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-N,N-diethylethanamine hydrobromide (1069-72-3) → 2-(diethylamino)ethyl bromide (5392-81-4)

Guidance literature:

With water; sodium carbonate; In ethyl acetate;

Reference yield:

2-(Diethylamino)ethanol (100-37-8) → 2-(diethylamino)ethyl bromide (5392-81-4)

Guidance literature:

With hydrogen bromide;

DOI:10.1021/ja01265a502 DOI:10.1007/BF03263127

Reference yield:

→ 2-(diethylamino)ethyl bromide (5392-81-4)

Guidance literature:

With hydrogen bromide; at 130 - 135 ℃;

upstream raw materials:

2-(Diethylamino)ethanol

ethylene dibromide

2-bromo-N,N-diethylethanamine hydrobromide

Downstream raw materials:

4-(2-(diethylamino)ethoxy)-3-methoxybenzaldehyde

C₆H₄(NHCH₂CH₂N(C₂H₅)2)NNC₆H₄CH₃

C₆H₄(NHCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl

C₆H₄(NHCH₂CH₂N(C₂H₅)2)NNC₆H₅

Refernces

• 1、 Cook,Kreke. "-". . p. 2971. Retrieved 1939.