N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide
CAS No.:112970-57-7
Molecular Formula:C13H11 Br2 N O2 S
Molecular Weight:405.1049
Hs Code.:
DSSTox Substance ID:DTXSID80382715
Wikidata:Q82174103

Synonyms:ST50939925;N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide;DTXSID80382715;STK444668;AKOS003290486;112970-57-7

Suppliers and Price of N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide

Chemical Property:

Vapor Pressure:9.06E-09mmHg at 25°C
Boiling Point:463.5°Cat760mmHg
Flash Point:234.1°C
Density:1.783g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:404.88568
Heavy Atom Count:19
Complexity:388

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2=C(C=C(C=C2)Br)Br

Technology Process of N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(2,4-dibromophenyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 615-57-6
2,4-dibromo-aniline

: 98-59-9
p-toluenesulfonyl chloride

: 112970-57-7
2,4-dibromo-N-tosylaniline

Guidance literature:: In pyridine; for 6h; Ambient temperature;
DOI:10.1021/jo00241a010

Reference yield:

: 420-90-6
3-bromo-3,3-difluropropene

: 112970-57-7
2,4-dibromo-N-tosylaniline

: C₁₆H₁₃Br₂F₂NO₂S

: C₁₆H₁₃Br₂F₂NO₂S

Guidance literature:: 2,4-dibromo-N-tosylaniline; With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; In diethyl ether; hexane; at -78 - 20 ℃; for 0.333333h; Inert atmosphere;

3-bromo-3,3-difluropropene; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In diethyl ether; hexane; at 0 ℃; for 0.5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03390

Reference yield:

: 112970-57-7
2,4-dibromo-N-tosylaniline

: potassium vinyltrifluoroborate

: C₁₅H₁₄BrNO₂S

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine; In methanol; Inert atmosphere; Reflux;
DOI:10.1021/acs.orglett.9b01362