4-Benzyloxy-2,3-dimethyl-butan-2-OL

Base Information

Chemical Name:4-Benzyloxy-2,3-dimethyl-butan-2-OL
CAS No.:93748-46-0
Molecular Formula:C13H20O2
Molecular Weight:208.29700
Hs Code.:2909499000
DSSTox Substance ID:DTXSID60441410
Mol file:93748-46-0.mol

Synonyms:4-BENZYLOXY-2,3-DIMETHYL-BUTAN-2-OL;93748-46-0;2,3-dimethyl-4-phenylmethoxybutan-2-ol;DTXSID60441410

Suppliers and Price of 4-Benzyloxy-2,3-dimethyl-butan-2-OL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Benzyloxy-2,3-dimethyl-butan-2-OL

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:317.398oC at 760 mmHg
PKA:14.94±0.29(Predicted)
Flash Point:128.389oC
PSA：29.46000
Density:0.996g/cm3
LogP:2.61020
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:208.146329876
Heavy Atom Count:15
Complexity:171

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(COCC1=CC=CC=C1)C(C)(C)O

Technology Process of 4-Benzyloxy-2,3-dimethyl-butan-2-OL

There total 3 articles about 4-Benzyloxy-2,3-dimethyl-butan-2-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 71312-15-7,93748-45-9,131423-76-2
1-benzyloxy-2,3-epoxy-3-methylbutane

: 93748-46-0
(S)-4-Benzyloxy-2,3-dimethyl-butan-2-ol

Guidance literature:: In diethyl ether; at -20 ℃;
DOI:10.1016/S0040-4039(01)81381-2

Reference yield:

: 62748-09-8
[(2R)-3,3-dimethyloxiran-2-yl]methanol

: 93748-46-0
(S)-4-Benzyloxy-2,3-dimethyl-butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaH / dimethylsulfoxide / Ambient temperature

2: 93 percent / diethyl ether / -20 °C

With sodium hydride; In diethyl ether; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)81381-2

Reference yield:

: 556-82-1
3-methyl-2-buten-1-ol

: 93748-46-0
(S)-4-Benzyloxy-2,3-dimethyl-butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / tert-butylhydroperoxide, titanium(IV) isopropoxyde, D-(-)-dibutyl tartarate / CH₂Cl₂ / -20 °C

2: 92 percent / NaH / dimethylsulfoxide / Ambient temperature

3: 93 percent / diethyl ether / -20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hydride; (2S,3S)-dibutyl 2,3-dihydroxysuccinate; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)81381-2