Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)-

Base Information

Chemical Name:Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)-
CAS No.:93768-83-3
Molecular Formula:C15H18
Molecular Weight:198.308
Hs Code.:

Synonyms:phenyltetramethylcyclopentadiene;Phenyltetramethylcyclopentadien;1-phenyl-2,3,4,5-tetramethyl-2,4-cyclopentadiene;

Suppliers and Price of Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)-

Chemical Property:

PSA：0.00000
LogP:4.45660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)-

There total 4 articles about Benzene, (2,3,4,5-tetramethyl-2,4-cyclopentadien-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 54458-61-6
2,3,4,5-tetramethyl-2-cyclopenten-1-one

: 100-58-3
phenylmagnesium bromide

: 93768-83-3
(2,3,4,5-tetramethylcyclopenta-2,4-dien-1-yl)-benzene

Guidance literature:: In tetrahydrofuran; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/acs.organomet.6b00580

Reference yield: 88.0%

: 503-17-3
dimethylacetylene

: 87-85-4
Hexamethylbenzene

: 93768-83-3
(2,3,4,5-tetramethylcyclopenta-2,4-dien-1-yl)-benzene

Guidance literature:: With Ti(pyridine-2,6-bis(4,6-di-tert-butylphenolate))(Bn)₂; In benzene-d6; at 90 ℃; for 1h; Catalytic behavior; Sealed tube; Inert atmosphere; Glovebox; Schlenk technique;
DOI:10.1021/om400080g