1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane

Base Information

Chemical Name:1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane
CAS No.:93885-42-8
Molecular Formula:C10H12O2
Molecular Weight:164.204
Hs Code.:
DSSTox Substance ID:DTXSID401285562

Synonyms:1-(2-hydroxyphenyl)-2-methyl-2,3-epoxypropane;93885-42-8;SCHEMBL10975542;ARVBHJORNGLFAF-UHFFFAOYSA-N;DTXSID401285562;2-[(2-Methyl-2-oxiranyl)methyl]phenol

Suppliers and Price of 1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:164.083729621
Heavy Atom Count:12
Complexity:169

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CO1)CC2=CC=CC=C2O

Technology Process of 1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane

There total 3 articles about 1-(2-Hydroxyphenyl)-2-methyl-2,3-epoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 20944-88-1
2-(methylallyl)phenol

: 93885-42-8
1-(2-hydroxyphenyl)-2-methyl-2,3-epoxypropane

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In dichloromethane; at 40 ℃; for 1.5h;
DOI:10.1055/s-2002-31894

Reference yield:

: 5820-22-4
methylallyl phenyl ether

: 93885-42-8
1-(2-hydroxyphenyl)-2-methyl-2,3-epoxypropane

Guidance literature:: Multi-step reaction with 2 steps

1: 0.17 h / 245 - 250 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / 10 - 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00371a003

Reference yield:

: 108-95-2,27073-41-2
phenol

: 93885-42-8
1-(2-hydroxyphenyl)-2-methyl-2,3-epoxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 1.) 3 h, 2.) 60 - 65 deg C, 3 h, 3.) RT, overnight

2: 0.17 h / 245 - 250 °C

3: m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / 10 - 20 °C

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00371a003