1,2-Dimethoxy-1,2-dihydroacenaphthylene

Base Information

Chemical Name:1,2-Dimethoxy-1,2-dihydroacenaphthylene
CAS No.:93911-23-0
Molecular Formula:C14H14O2
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID00523269
Nikkaji Number:J833.117K

Synonyms:1,2-DIMETHOXY-1,2-DIHYDROACENAPHTHYLENE;1,2-Dimethoxyacenaphthene;93911-23-0;DTXSID00523269

Suppliers and Price of 1,2-Dimethoxy-1,2-dihydroacenaphthylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Dimethoxy-1,2-dihydroacenaphthylene

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:214.099379685
Heavy Atom Count:16
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1C(C2=CC=CC3=C2C1=CC=C3)OC

Technology Process of 1,2-Dimethoxy-1,2-dihydroacenaphthylene

There total 6 articles about 1,2-Dimethoxy-1,2-dihydroacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2963-87-3
trans-1,2-acenaphthalenediol

: 74-88-4
methyl iodide

: 42211-51-8,42314-31-8,93911-23-0
E-1,2-dihydro-1,2-dimethoxyacenaphthylene

Guidance literature:: With potassium tert-butylate; In 1,4-dioxane; tert-butyl alcohol; water bath heating;

Reference yield: 67.0%

: 76177-02-1,76177-03-2
trans-2-methoxy-1-acenaphthenol

: 74-88-4
methyl iodide

: 42211-51-8,42314-31-8,93911-23-0
E-1,2-dihydro-1,2-dimethoxyacenaphthylene

Guidance literature:: With potassium tert-butylate; In diethyl ether; tert-butyl alcohol; water bath heating;

Reference yield:

: 2963-87-3
trans-1,2-acenaphthalenediol

: 77-78-1
dimethyl sulfate

: 42211-51-8,42314-31-8,93911-23-0
E-1,2-dihydro-1,2-dimethoxyacenaphthylene

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In 1,4-dioxane; at 80 ℃; for 1.5h; Yield given;
DOI:10.1016/S0040-4020(01)91094-4