Acetamide, N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl]-

Base Information

• Chemical Name: Acetamide, N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl]-
• CAS No.: 93929-04-5
• Molecular Formula: C₁₁H₁₂N₂O₅
• Molecular Weight: 252.227

Synonyms:N-[1-hydroxymethyl-2-(2-nitro-phenyl)-2-oxo-ethyl]-acetamide;Acetamide,N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl];N-[1-Hydroxymethyl-2-(2-nitro-phenyl)-2-oxo-aethyl]-acetamid;(+-)-2-Acetylamino-3-hydroxy-1-(2-nitro-phenyl)-propan-1-on;

Chemical Property of Acetamide, N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl]-

Chemical Property:

• Melting Point: 126-127 °C
• Boiling Point: 568.4±50.0 °C(Predicted)
• PSA: 115.71000
• Density: 1.354±0.06 g/cm3(Predicted)
• LogP: 1.63800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetamide, N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl]-

There total 2 articles about Acetamide, N-[1-(hydroxymethyl)-2-(2-nitrophenyl)-2-oxoethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-1-(2-nitrophenyl)ethanone (6851-99-6) → N-[1-hydroxymethyl-2-(2-nitro-phenyl)-2-oxo-ethyl]-acetamide (93929-04-5)

Guidance literature:

Multi-step reaction with 2 steps

2: NaHCO₃; Na₂CO₃; aqueous methanol

With methanol; sodium hydrogencarbonate; sodium carbonate;

DOI:10.1021/ja01165a530

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-(2-nitro-phenacyl)-acetamide (163464-74-2) → N-[1-hydroxymethyl-2-(2-nitro-phenyl)-2-oxo-ethyl]-acetamide (93929-04-5)

Guidance literature:

With methanol; sodium hydrogencarbonate; sodium carbonate;

DOI:10.1021/ja01165a530

Reference yield:

N-[1-hydroxymethyl-2-(2-nitro-phenyl)-2-oxo-ethyl]-acetamide (93929-04-5) → N-[(1RS,2RS)-2-hydroxy-1-hydroxymethyl-2-(2-nitro-phenyl)-ethyl]-acetamide

Guidance literature:

With aluminum isopropoxide; isopropyl alcohol;

DOI:10.1021/ja01165a530

upstream raw materials:

formaldehyd

N-(2-nitro-phenacyl)-acetamide

2-bromo-1-(2-nitrophenyl)ethanone

Downstream raw materials:

dichloroacetic acid-[(1RS,2RS)-2-hydroxy-1-hydroxymethyl-2-(2-nitro-phenyl)-ethylamide]

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