5-(4-chlorobenzylidene)-2-(phenylimino)-1,3-thiazolidin-4-one

Base Information

Chemical Name:5-(4-chlorobenzylidene)-2-(phenylimino)-1,3-thiazolidin-4-one
CAS No.:93989-47-0
Molecular Formula:C16H11ClN2OS
Molecular Weight:314.795
Hs Code.:
Mol file:93989-47-0.mol

Synonyms:5-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-2-phenylamino-thiazol-4-one;2-Anilino-5-(4-chlor-benzyliden)-thiazol-4-on;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-chlorobenzylidene)-2-(phenylimino)-1,3-thiazolidin-4-one

Chemical Property:

Melting Point:290 °C (acetic acid)
PSA：66.76000
LogP:3.93100

Purity/Quality:

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Technology Process of 5-(4-chlorobenzylidene)-2-(phenylimino)-1,3-thiazolidin-4-one

There total 4 articles about 5-(4-chlorobenzylidene)-2-(phenylimino)-1,3-thiazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 104-88-1
4-chlorobenzaldehyde

: 17823-27-7
2-(phenylimino)thiazolidin-4-one

: 93989-47-0
5-(4-chlorobenzylidene)-2-(phenylimino)thiazolidin-4-one

Guidance literature:: With sodium acetate; acetic acid; for 72h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2016.04.075

Reference yield:

: 103-85-5
monophenylthiourea

: 93989-47-0
5-(4-chlorobenzylidene)-2-(phenylimino)thiazolidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / ethanol / 6 h / Reflux; Inert atmosphere

2: sodium acetate; acetic acid / 72 h / Reflux; Inert atmosphere

With sodium acetate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2016.04.075

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 93989-47-0
5-(4-chlorobenzylidene)-2-(phenylimino)thiazolidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / dichloromethane; water / 2 h / 20 °C / Inert atmosphere

2: sodium acetate / ethanol / 6 h / Reflux; Inert atmosphere

3: sodium acetate; acetic acid / 72 h / Reflux; Inert atmosphere

With ammonium hydroxide; sodium acetate; acetic acid; In ethanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2016.04.075