1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone

Base Information

Chemical Name:1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone
CAS No.:94190-88-2
Molecular Formula:C14H18O6
Molecular Weight:282.293
Hs Code.:
Mol file:94190-88-2.mol

Synonyms:1-[2-Hydroxy-4,6-dimethoxy-3-(1-oxopropoxy)phenyl]-1-propanone;

Suppliers and Price of 1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-[2-Hydroxy-4,6-dimethoxy-3-(1-oxopropoxy)phenyl]-1-propanone
1g
$ 1455.00

Medical Isotopes, Inc.
1-[2-Hydroxy-4,6-dimethoxy-3-(1-oxopropoxy)phenyl]-1-propanone
1 g
$ 2200.00

Total 4 raw suppliers

Chemical Property of 1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone

Chemical Property:

Melting Point:119 - 124°C
Boiling Point:418.6±45.0 °C (760 mmHg)
PSA：82.06000
Density:1.185±0.06 g/cm3(20 °C , 760mmHg)
LogP:2.31750
Storage Temp.:Hygroscopic, -20°C Freezer, Under inert atmosphere
Solubility.:Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:: 1-[2-Hydroxy-4,6-dimethoxy-3-(1-oxopropoxy)phenyl]-1-propanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 1-[2-Hydroxy-4,6-dimethoxy-3-(1-oxopropoxy)phenyl]-1-propanone is a reactant used in the preparation of Stigmatellin A (S686780).

Technology Process of 1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone

There total 2 articles about 1-[2-Hydroxy-4,6-diMethoxy-3-(1-oxopropoxy)phenyl]-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 94190-87-1
1-(2-Hydroxy-4,6-dimethoxy-3-propionylphenyl)-1-propanone

: 94190-88-2
Propionic acid 2-hydroxy-4,6-dimethoxy-3-propionylphenyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; at 0 - 5 ℃; for 16h;

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 94190-88-2
Propionic acid 2-hydroxy-4,6-dimethoxy-3-propionylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / P₄O₁₀; H₃PO₄ / 1 h / 70 °C

2: 87 percent / TFA; MCPBA / CH₂Cl₂ / 16 h / 0 - 5 °C

With phosphorus pentoxide; phosphoric acid; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; 1: Acylation / 2: Baeyer-Villiger oxidation;