Technology Process of 1,2,4,3,5-Dithiazadiborolidine, 3,5-dibromo-4-phenyl-
There total 1 articles about 1,2,4,3,5-Dithiazadiborolidine, 3,5-dibromo-4-phenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
tetrachloromethane;
dropwise addn. of equimolar amt. of the azomethine soln. to stirred soln. of the diborolane in CCl4 (N2, room temp., 15 min), refluxed (20 h); evapn. (high vac.), distn.; oil; elem. anal.;
- Guidance literature:
-
In
hexane;
byproducts: (C2H5)2NH2Br; addn. of Li compd. to dithiazadiborolidine in n-hexane under N2, warming to room temp. and refluxing for 4 h; decantation, sepn. of the solvent and distn. (high vac.); elem. anal.;
- Guidance literature:
-
In
hexane;
byproducts: ((CH3)2CH)2NH2Br; addn. of Li compd. to dithiazadiborolidine in n-hexane under N2, warming to room temp. and refluxing for 4 h; decantation, sepn. of the solvent and sublimation (high vac.); elem. anal.;
