2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid

Base Information

Chemical Name:2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid
CAS No.:76981-42-5
Molecular Formula:C17H14Cl2O4
Molecular Weight:353.1967
Hs Code.:
DSSTox Substance ID:DTXSID00998256
Nikkaji Number:J92.663I

Synonyms:BRN 5609681;2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid;Propionic acid, 2-(3-(3,4-dichlorobenzoyl)-o-tolyloxy)-;76981-42-5;2-[3-(3,4-Dichlorobenzoyl)-o-tolyloxy]propionic acid;2-[3-(3,4-dichlorobenzoyl)-2-methylphenoxy]propanoic acid;DTXSID00998256;LS-124620

Suppliers and Price of 2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid

Chemical Property:

Vapor Pressure:4.69E-11mmHg at 25°C
Boiling Point:505.9°Cat760mmHg
Flash Point:259.7°C
Density:1.359g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:352.0269143
Heavy Atom Count:23
Complexity:442

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC=C1OC(C)C(=O)O)C(=O)C2=CC(=C(C=C2)Cl)Cl

Technology Process of 2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid

There total 6 articles about 2-(3-(3,4-Dichlorobenzoyl)-o-tolyloxy)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 76981-64-1
2-[3-(3,4-Dichloro-benzoyl)-2-methyl-phenoxy]-propionic acid ethyl ester

: 76981-42-5
2-[3-(3,4-Dichloro-benzoyl)-2-methyl-phenoxy]-propionic acid

Guidance literature:: With water; sodium carbonate; In ethanol; Ambient temperature;

Reference yield:

: 39053-41-3
2-methyl-3-nitrobenzoyl chloride

: 76981-42-5
2-[3-(3,4-Dichloro-benzoyl)-2-methyl-phenoxy]-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 52.5 percent / aluminium trichloride / 2 h / 100 °C

2: 66 percent / SnCl₂, HCl / 2 h / Heating

3: 1.) 5 N sulfuric acid, sodium nitrite, 2.) CuSO₄, water / 1.) water, 0-5 deg C, 30 min, 2.) heating

4: 72 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C

5: 72 percent / 1.) H₂O, sodium carbonate, 2.) acid / ethanol / Ambient temperature

With hydrogenchloride; aluminium trichloride; sulfuric acid; water; sodium carbonate; potassium carbonate; copper(II) sulfate; tin(ll) chloride; sodium nitrite; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 76981-65-2
(3,4-Dichloro-phenyl)-(3-hydroxy-2-methyl-phenyl)-methanone

: 76981-42-5
2-[3-(3,4-Dichloro-benzoyl)-2-methyl-phenoxy]-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C

2: 72 percent / 1.) H₂O, sodium carbonate, 2.) acid / ethanol / Ambient temperature

With water; sodium carbonate; potassium carbonate; In ethanol; N,N-dimethyl-formamide;