5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid, 6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-, 1,1-dimethylethyl ester, 6-oxide

Base Information

Chemical Name:5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid, 6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-, 1,1-dimethylethyl ester, 6-oxide
CAS No.:94472-25-0
Molecular Formula:C50H87BrNO11P
Molecular Weight:989.119
Hs Code.:

5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid,
6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-,
1,1-dimethylethyl ester, 6-oxide

Synonyms:

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Chemical Property of 5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid, 6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-, 1,1-dimethylethyl ester, 6-oxide

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Technology Process of 5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid, 6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-, 1,1-dimethylethyl ester, 6-oxide

There total 3 articles about 5,7,11-Trioxa-2-aza-6-phosphaheptacosanoic acid, 6-[2-(4-bromophenyl)-2-oxoethoxy]-12-oxo-9-[(1-oxohexadecyl)oxy]-, 1,1-dimethylethyl ester, 6-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 94482-99-2
phosphonate hydroxyl

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 94472-25-0
Hexadecanoic acid 2-[[2-(4-bromo-phenyl)-2-oxo-ethoxy]-(2-tert-butoxycarbonylamino-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 22 ℃; for 20h;
DOI:10.1016/S0040-4039(00)83994-5

Reference yield:

: 5681-36-7,3026-45-7
1,2-dipalmitoyl-sn-glycero-3-phospoethanolamine

: 94472-25-0
Hexadecanoic acid 2-[[2-(4-bromo-phenyl)-2-oxo-ethoxy]-(2-tert-butoxycarbonylamino-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Et₃N / dioxane; H₂O / 3 h / 55 °C

2: 60 percent / Et₃N / dimethylformamide; tetrahydrofuran / 20 h / 22 °C

With triethylamine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)83994-5

Reference yield:

: C₅H₉NO₄

: 94472-25-0
Hexadecanoic acid 2-[[2-(4-bromo-phenyl)-2-oxo-ethoxy]-(2-tert-butoxycarbonylamino-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Et₃N / dioxane; H₂O / 3 h / 55 °C

2: 60 percent / Et₃N / dimethylformamide; tetrahydrofuran / 20 h / 22 °C

With triethylamine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)83994-5