L-Tyrosine, O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[ (1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5- diiodo-

Base Information

Chemical Name:L-Tyrosine, O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[ (1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5- diiodo-
CAS No.:94491-16-4
Molecular Formula:C56H87I4N2O14P
Molecular Weight:1550.9
Hs Code.:

L-Tyrosine,
O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[
(1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5-
diiodo-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Tyrosine, O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[ (1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5- diiodo-

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MSDS Files:: SDS file from LookChem

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Technology Process of L-Tyrosine, O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[ (1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5- diiodo-

There total 8 articles about L-Tyrosine, O-(4-hydroxy-3,5-diiodophenyl)-N-[9-hydroxy-9-oxido-1,4,15-trioxo-12-[ (1-oxohexadecyl)oxy]-8,10,14-trioxa-5-aza-9-phosphatriacont-1-yl]-3,5- diiodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 94451-78-2
Hexadecanoic acid 2-{[2-(4-bromo-phenyl)-2-oxo-ethoxy]-[2-(3-{(S)-1-carboxy-2-[4-(4-hydroxy-3,5-diiodo-phenoxy)-3,5-diiodo-phenyl]-ethylcarbamoyl}-propionylamino)-ethoxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

: 94491-16-4
Hexadecanoic acid 2-{[2-(3-{(S)-1-carboxy-2-[4-(4-hydroxy-3,5-diiodo-phenoxy)-3,5-diiodo-phenyl]-ethylcarbamoyl}-propionylamino)-ethoxy]-hydroxy-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 22 ℃; for 2h;
DOI:10.1016/S0040-4039(00)83994-5

Reference yield:

: 5681-36-7,3026-45-7
1,2-dipalmitoyl-sn-glycero-3-phospoethanolamine

: 94491-16-4
Hexadecanoic acid 2-{[2-(3-{(S)-1-carboxy-2-[4-(4-hydroxy-3,5-diiodo-phenoxy)-3,5-diiodo-phenyl]-ethylcarbamoyl}-propionylamino)-ethoxy]-hydroxy-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / Et₃N / dioxane; H₂O / 3 h / 55 °C

2: 60 percent / Et₃N / dimethylformamide; tetrahydrofuran / 20 h / 22 °C

3: 30percent TFA / CH₂Cl₂ / 0.5 h

4: 44 percent / dimethylformamide; CHCl₃ / 3 h / 55 °C

5: 1.) DCC / 1.) CH₂Cl₂, 22 deg C, 0.1 h 2.) DMF, 22 deg C, 4 h

6: 52 percent / DBU / CHCl₃ / 2 h / 22 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)83994-5

Reference yield:

: 94451-70-4
Hexadecanoic acid 2-{(2-amino-ethoxy)-[2-(4-bromo-phenyl)-2-oxo-ethoxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

: 94491-16-4
Hexadecanoic acid 2-{[2-(3-{(S)-1-carboxy-2-[4-(4-hydroxy-3,5-diiodo-phenoxy)-3,5-diiodo-phenyl]-ethylcarbamoyl}-propionylamino)-ethoxy]-hydroxy-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 44 percent / dimethylformamide; CHCl₃ / 3 h / 55 °C

2: 1.) DCC / 1.) CH₂Cl₂, 22 deg C, 0.1 h 2.) DMF, 22 deg C, 4 h

3: 52 percent / DBU / CHCl₃ / 2 h / 22 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)83994-5