Benzenamine, N,N-diethyl-4-(2-methoxy-1-methylethyl)-

Base Information

Chemical Name:Benzenamine, N,N-diethyl-4-(2-methoxy-1-methylethyl)-
CAS No.:94474-90-5
Molecular Formula:C₁₄H₂₃NO
Molecular Weight:221.343
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, N,N-diethyl-4-(2-methoxy-1-methylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenamine, N,N-diethyl-4-(2-methoxy-1-methylethyl)-

There total 4 articles about Benzenamine, N,N-diethyl-4-(2-methoxy-1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34713-70-7
2-Phenylpropanal

: 94474-90-5
2-p-N,N-diethylaminophenyl-1-propyl methyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / sodium borohydride, 2 M NaOH / ethanol; H₂O / Ambient temperature

2: 75 percent / 1.) tetrabutylammonium iodide, 12 M NaOH / 1.) petroleum ether, 30 min; 2.) 4 h

3: 40 percent / nitric acid, sulphuric acid / 4 h / -15 °C

4: 1.) stannous chloride dihydrate; 2.) 15percent KOH / 1.) abs. ethanol, reflux, 4 h; 2.) 48 h

5: 1.) lithium bromide; 2.) 1.25M NaOH / 1.) reflux, 4 h; 2.) reflux, 1 h

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; sulfuric acid; nitric acid; tetra-(n-butyl)ammonium iodide; tin(ll) chloride; lithium bromide; In ethanol; water;
DOI:10.1016/S0040-4020(01)87425-1

Reference yield:

: 1123-85-9
(RS)-2-phenyl-1-propanol

: 94474-90-5
2-p-N,N-diethylaminophenyl-1-propyl methyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / 1.) tetrabutylammonium iodide, 12 M NaOH / 1.) petroleum ether, 30 min; 2.) 4 h

2: 40 percent / nitric acid, sulphuric acid / 4 h / -15 °C

3: 1.) stannous chloride dihydrate; 2.) 15percent KOH / 1.) abs. ethanol, reflux, 4 h; 2.) 48 h

4: 1.) lithium bromide; 2.) 1.25M NaOH / 1.) reflux, 4 h; 2.) reflux, 1 h

With potassium hydroxide; sodium hydroxide; sulfuric acid; nitric acid; tetra-(n-butyl)ammonium iodide; tin(ll) chloride; lithium bromide;
DOI:10.1016/S0040-4020(01)87425-1

Reference yield:

: 65738-46-7
2-phenyl-1-propyl methyl ether

: 94474-90-5
2-p-N,N-diethylaminophenyl-1-propyl methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / nitric acid, sulphuric acid / 4 h / -15 °C

2: 1.) stannous chloride dihydrate; 2.) 15percent KOH / 1.) abs. ethanol, reflux, 4 h; 2.) 48 h

3: 1.) lithium bromide; 2.) 1.25M NaOH / 1.) reflux, 4 h; 2.) reflux, 1 h

With potassium hydroxide; sodium hydroxide; sulfuric acid; nitric acid; tin(ll) chloride; lithium bromide;
DOI:10.1016/S0040-4020(01)87425-1